4-ethyl-1-(phenylsulfonyl)-1,3,4,5-tetrahydropyrrolo[4,3,2-de]isoquinoline trifluoroacetate

Base Information

Chemical Name:4-ethyl-1-(phenylsulfonyl)-1,3,4,5-tetrahydropyrrolo[4,3,2-de]isoquinoline trifluoroacetate
CAS No.:1059128-98-1
Molecular Formula:C₂HF₃O₂*C₁₈H₁₈N₂O₂S
Molecular Weight:440.443
Hs Code.:

Synonyms:4-ethyl-1-(phenylsulfonyl)-1,3,4,5-tetrahydropyrrolo[4,3,2-de]isoquinoline trifluoroacetate

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Chemical Property of 4-ethyl-1-(phenylsulfonyl)-1,3,4,5-tetrahydropyrrolo[4,3,2-de]isoquinoline trifluoroacetate

Chemical Property:

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Technology Process of 4-ethyl-1-(phenylsulfonyl)-1,3,4,5-tetrahydropyrrolo[4,3,2-de]isoquinoline trifluoroacetate

There total 8 articles about 4-ethyl-1-(phenylsulfonyl)-1,3,4,5-tetrahydropyrrolo[4,3,2-de]isoquinoline trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1059128-86-7
1-(phenylsulfonyl)-1,3,4,5-tetrahydropyrrolo[4,3,2-de]isoquinoline

: 75-07-0,9002-91-9
acetaldehyde

: 76-05-1
trifluoroacetic acid

: 1059128-98-1
4-ethyl-1-(phenylsulfonyl)-1,3,4,5-tetrahydropyrrolo[4,3,2-de]isoquinoline trifluoroacetate

Guidance literature:: 1-(phenylsulfonyl)-1,3,4,5-tetrahydropyrrolo[4,3,2-de]isoquinoline; acetaldehyde; With sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; at 130 ℃; for 0.2h; Microwave irradiation;

trifluoroacetic acid; In acetonitrile;

Reference yield:

: C₁₁H₁₀N₂O₃

: 1059128-98-1
4-ethyl-1-(phenylsulfonyl)-1,3,4,5-tetrahydropyrrolo[4,3,2-de]isoquinoline trifluoroacetate

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogen / palladium on activated charcoal

2: sodium methylate / methanol

3: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / dichloromethane; water / 2 h / 20 °C

4: dimethylsulfide borane complex / tetrahydrofuran / 20 °C / Heating / reflux

5: sodium tris(acetoxy)borohydride; acetic acid / tetrahydrofuran / 0.2 h / 130 °C / Microwave irradiation

With sodium hydroxide; dimethylsulfide borane complex; hydrogen; sodium methylate; tetra(n-butyl)ammonium hydrogensulfate; sodium tris(acetoxy)borohydride; acetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water;

Reference yield:

: 53462-88-7
3-Formylindole-4-carboxylic acid methyl ester

: 1059128-98-1
4-ethyl-1-(phenylsulfonyl)-1,3,4,5-tetrahydropyrrolo[4,3,2-de]isoquinoline trifluoroacetate

Guidance literature:: Multi-step reaction with 6 steps

1: hydroxylamine hydrochloride

2: hydrogen / palladium on activated charcoal

3: sodium methylate / methanol

4: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / dichloromethane; water / 2 h / 20 °C

5: dimethylsulfide borane complex / tetrahydrofuran / 20 °C / Heating / reflux

6: sodium tris(acetoxy)borohydride; acetic acid / tetrahydrofuran / 0.2 h / 130 °C / Microwave irradiation

With sodium hydroxide; dimethylsulfide borane complex; hydroxylamine hydrochloride; hydrogen; sodium methylate; tetra(n-butyl)ammonium hydrogensulfate; sodium tris(acetoxy)borohydride; acetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water;