1-(phenylsulfonyl)-1,3,4,5-tetrahydropyrrolo[4,3,2-de]isoquinoline

Base Information

Chemical Name:1-(phenylsulfonyl)-1,3,4,5-tetrahydropyrrolo[4,3,2-de]isoquinoline
CAS No.:1059128-86-7
Molecular Formula:C₁₆H₁₄N₂O₂S
Molecular Weight:298.365
Hs Code.:

Synonyms:1-(phenylsulfonyl)-1,3,4,5-tetrahydropyrrolo[4,3,2-de]isoquinoline

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Chemical Property of 1-(phenylsulfonyl)-1,3,4,5-tetrahydropyrrolo[4,3,2-de]isoquinoline

Chemical Property:

Purity/Quality:

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Technology Process of 1-(phenylsulfonyl)-1,3,4,5-tetrahydropyrrolo[4,3,2-de]isoquinoline

There total 7 articles about 1-(phenylsulfonyl)-1,3,4,5-tetrahydropyrrolo[4,3,2-de]isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1059131-08-6
1-(phenylsulfonyl)-3,4-dihydropyrrolo[4,3,2-de]isoquinolin-5(1H)-one

: 1059128-86-7
1-(phenylsulfonyl)-1,3,4,5-tetrahydropyrrolo[4,3,2-de]isoquinoline

Guidance literature:: With dimethylsulfide borane complex; In tetrahydrofuran; at 20 ℃; Heating / reflux;

Reference yield:

: 53462-88-7
3-Formylindole-4-carboxylic acid methyl ester

: 1059128-86-7
1-(phenylsulfonyl)-1,3,4,5-tetrahydropyrrolo[4,3,2-de]isoquinoline

Guidance literature:: Multi-step reaction with 5 steps

1: hydroxylamine hydrochloride

2: hydrogen / palladium on activated charcoal

3: sodium methylate / methanol

4: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / dichloromethane; water / 2 h / 20 °C

5: dimethylsulfide borane complex / tetrahydrofuran / 20 °C / Heating / reflux

With sodium hydroxide; dimethylsulfide borane complex; hydroxylamine hydrochloride; hydrogen; sodium methylate; tetra(n-butyl)ammonium hydrogensulfate; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water;

Reference yield:

: 93-61-8
N-methyl-N-phenylformamide

: 1059128-86-7
1-(phenylsulfonyl)-1,3,4,5-tetrahydropyrrolo[4,3,2-de]isoquinoline

Guidance literature:: Multi-step reaction with 6 steps

1: trichlorophosphate

2: hydroxylamine hydrochloride

3: hydrogen / palladium on activated charcoal

4: sodium methylate / methanol

5: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / dichloromethane; water / 2 h / 20 °C

6: dimethylsulfide borane complex / tetrahydrofuran / 20 °C / Heating / reflux

With sodium hydroxide; dimethylsulfide borane complex; hydroxylamine hydrochloride; hydrogen; sodium methylate; tetra(n-butyl)ammonium hydrogensulfate; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water;