tetrabromophenylstiborane

Base Information

Chemical Name:tetrabromophenylstiborane
CAS No.:130681-64-0
Molecular Formula:C₆H₅Br₄Sb
Molecular Weight:518.472
Hs Code.:

Synonyms:tetrabromophenylstiborane

Suppliers and Price of tetrabromophenylstiborane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetrabromophenylstiborane

Chemical Property:

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Technology Process of tetrabromophenylstiborane

There total 1 articles about tetrabromophenylstiborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 73046-27-2
dibromophenylantimony

: 7726-95-6
bromine

: 130681-64-0
tetrabromophenylstiborane

Guidance literature:: In dichloromethane; dropwise addn. of Br2 soln. to a soln. of PhSbBr2 (-78°C, exclusion of light), warmed to -30°C; evapn., dried (below 0°C, vac.); elem. anal.;

Reference yield: 85.0%

: 130681-64-0
tetrabromophenylstiborane

: 71-91-0
tetraethylammonium bromide

: tetraethylammonium pentabromophenylantimonate(V)

Guidance literature:: In dichloromethane; N2 atm.; exclusion of light, room temp.; addn. of petroleum ether (30-50°C), pptn., supernatant decanted, residue washed (petroleum ether), dried (vac.);