N-(3-bromo-4-chlorophenyl)-2-chloroacetamide

Base Information

Chemical Name:N-(3-bromo-4-chlorophenyl)-2-chloroacetamide
CAS No.:22459-87-6
Molecular Formula:C₈H₆BrCl₂NO
Molecular Weight:282.952
Hs Code.:

Synonyms:N-(3-bromo-4-chlorophenyl)-2-chloroacetamide

Suppliers and Price of N-(3-bromo-4-chlorophenyl)-2-chloroacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N-(3-bromo-4-chlorophenyl)-2-chloroacetamide

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Technology Process of N-(3-bromo-4-chlorophenyl)-2-chloroacetamide

There total 3 articles about N-(3-bromo-4-chlorophenyl)-2-chloroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 823-54-1
3-bromo-4-chloroaniline

: 79-04-9
chloroacetyl chloride

: 22459-87-6
N-(3-bromo-4-chlorophenyl)-2-chloroacetamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/acs.jmedchem.0c00021

Reference yield:

: 16588-26-4
3-bromo-4-chloronitrobenzene

: 22459-87-6
N-(3-bromo-4-chlorophenyl)-2-chloroacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium chloride; iron / water; ethanol / 16 h / 70 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

With iron; ammonium chloride; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane; water;
DOI:10.1021/acs.jmedchem.0c00021