[Mn₅O₃(tert-butylphosphonate)2(PhCOO)5(1,10-phenanthroline)2]*H₂O*(acetonitrile)

Base Information

• Chemical Name: [Mn₅O₃(tert-butylphosphonate)2(PhCOO)5(1,10-phenanthroline)2]*H₂O*(acetonitrile)
• CAS No.: 1037701-18-0
• Molecular Formula: C₂H₃N*C₆₇H₅₉Mn₅N₄O₁₉P₂*H₂O
• Molecular Weight: 1619.93

Synonyms:[Mn₅O₃(tert-butylphosphonate)2(PhCOO)5(1,10-phenanthroline)2]*H₂O*(acetonitrile)

Chemical Property of [Mn₅O₃(tert-butylphosphonate)2(PhCOO)5(1,10-phenanthroline)2]*H₂O*(acetonitrile)

Chemical Property:

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Technology Process of [Mn₅O₃(tert-butylphosphonate)2(PhCOO)5(1,10-phenanthroline)2]*H₂O*(acetonitrile)

There total 1 articles about [Mn₅O₃(tert-butylphosphonate)2(PhCOO)5(1,10-phenanthroline)2]*H₂O*(acetonitrile) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

1,10-Phenanthroline (66-71-7) + tetra-n-butylammonium permanganate (35638-41-6) + manganese(II) benzoate dihydrate + tert-butylphosphonic acid (4923-84-6) + benzoic acid (65-85-0,8013-63-6) → [Mn5O3(tert-butylphosphonate)2(PhCOO)5(1,10-phenanthroline)2]*H2O*(acetonitrile) (1037701-18-0)

Guidance literature:

With MeCN; In methanol; dichloromethane; acetonitrile; solid Bu4NMnO4 added in small portions to stirred soln. of Mn(O2CPh)2*2H2O and PhCOOH in MeCN-CH2Cl2; soln. of phenanthroline and t-BuPO(OH)2 inMeOH added; stirred at room temp. for 24 h; filtered; filtrate stored at room temp. for ca. 1 wk; crystals isolated;elem. anal.;

DOI:10.1021/ic701343s

upstream raw materials:

1,10-Phenanthroline

tetra-n-butylammonium permanganate

tert-butylphosphonic acid

benzoic acid

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