4,11-dimethyl-15-[(Z)-phenylmethylidene]-7,14-dioxadispiro[5.1.5.2]pentadecane

Base Information

Chemical Name:4,11-dimethyl-15-[(Z)-phenylmethylidene]-7,14-dioxadispiro[5.1.5.2]pentadecane
CAS No.:1316096-36-2
Molecular Formula:C₂₂H₃₀O₂
Molecular Weight:326.479
Hs Code.:

Synonyms:4,11-dimethyl-15-[(Z)-phenylmethylidene]-7,14-dioxadispiro[5.1.5.2]pentadecane

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Chemical Property of 4,11-dimethyl-15-[(Z)-phenylmethylidene]-7,14-dioxadispiro[5.1.5.2]pentadecane

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Technology Process of 4,11-dimethyl-15-[(Z)-phenylmethylidene]-7,14-dioxadispiro[5.1.5.2]pentadecane

There total 2 articles about 4,11-dimethyl-15-[(Z)-phenylmethylidene]-7,14-dioxadispiro[5.1.5.2]pentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 589-92-4
1-methylcyclohexan-4-one

: 536-74-3
phenylacetylene

: C₁₅H₁₈O

: C₁₅H₁₈O

: 1316096-36-2
4,11-dimethyl-15-[(Z)-phenylmethylidene]-7,14-dioxadispiro[5.1.5.2]pentadecane

Guidance literature:: With water; In dimethyl sulfoxide; at 80 ℃; for 1h; stereoselective reaction;
DOI:10.1016/j.tetlet.2011.05.056

Reference yield:

: 20109-09-5
1-(phenylethynyl)-1-cyclohexanol

: C₁₅H₁₈O

: C₁₅H₁₈O

: 1316096-36-2
4,11-dimethyl-15-[(Z)-phenylmethylidene]-7,14-dioxadispiro[5.1.5.2]pentadecane

Guidance literature:: Multi-step reaction with 2 steps

1: water / dimethyl sulfoxide / 1 h / 80 °C

2: water / dimethyl sulfoxide / 1 h / 80 °C

With water; In dimethyl sulfoxide;
DOI:10.1016/j.tetlet.2011.05.056