(3,5-diphenyl-1H-pyrrol-2-yl)-[3-(4-morpholin-4-ylmethylphenyl)-5-phenylpyrrol-2-ylidene]-amine BF₂ chelate

Base Information

• Chemical Name: (3,5-diphenyl-1H-pyrrol-2-yl)-[3-(4-morpholin-4-ylmethylphenyl)-5-phenylpyrrol-2-ylidene]-amine BF₂ chelate
• CAS No.: 884307-49-7
• Molecular Formula: C₃₇H₃₁BF₂N₄O
• Molecular Weight: 596.487

Synonyms:(3,5-diphenyl-1H-pyrrol-2-yl)-[3-(4-morpholin-4-ylmethylphenyl)-5-phenylpyrrol-2-ylidene]-amine BF₂ chelate

Chemical Property of (3,5-diphenyl-1H-pyrrol-2-yl)-[3-(4-morpholin-4-ylmethylphenyl)-5-phenylpyrrol-2-ylidene]-amine BF₂ chelate

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Technology Process of (3,5-diphenyl-1H-pyrrol-2-yl)-[3-(4-morpholin-4-ylmethylphenyl)-5-phenylpyrrol-2-ylidene]-amine BF₂ chelate

There total 1 articles about (3,5-diphenyl-1H-pyrrol-2-yl)-[3-(4-morpholin-4-ylmethylphenyl)-5-phenylpyrrol-2-ylidene]-amine BF₂ chelate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

(3,5-diphenyl-1H-pyrrol-2-yl)-[3-(4-morpholin-4-ylmethylphenyl)-5-phenylpyrrol-2-ylidene]-amine (862201-45-4) + trifluoroborane diethyl ether (109-63-7) → (3,5-diphenyl-1H-pyrrol-2-yl)-[3-(4-morpholin-4-ylmethylphenyl)-5-phenylpyrrol-2-ylidene]-amine BF2 chelate (884307-49-7)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; stirred soln. of ligand in CH2Cl2 treated with BF3*OEt2 and EtN(i-Pr)2; stirred at room temp. for 16 h; washed with H2O; dried over Na2SO4; solvent removed under reduced pressure; purified by chromy. (silica gel, EtOAc-cyclohexane 2:1);

DOI:10.1039/b514788c

Reference yield:

(3,5-diphenyl-1H-pyrrol-2-yl)-[3-(4-morpholin-4-ylmethylphenyl)-5-phenylpyrrol-2-ylidene]-amine BF2 chelate (884307-49-7) + trifluoroacetic acid (76-05-1) → BF2(NC(C6H5)CHC(C6H5)CNCC(C6H4CH2N(CH2CH2)2O)CHCC6H5N)*H(1+)=BF2(C37H32N4O)(1+)

Guidance literature:

In tetrahydrofuran; CF3COOH added to B compd. in THF; not isolated; detd. by UV-vis and fluorescence spectra;

DOI:10.1039/b514788c

upstream raw materials:

(3,5-diphenyl-1H-pyrrol-2-yl)-[3-(4-morpholin-4-ylmethylphenyl)-5-phenylpyrrol-2-ylidene]-amine

trifluoroborane diethyl ether

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