5-<3,5-bis(1,1-dimethylethyl)-4-<(2-methoxyethoxy)methoxy>phenyl>-1,3,4-thiadiazole-2(3H)-thione

Base Information

Chemical Name:5-<3,5-bis(1,1-dimethylethyl)-4-<(2-methoxyethoxy)methoxy>phenyl>-1,3,4-thiadiazole-2(3H)-thione
CAS No.:130116-75-5
Molecular Formula:C₂₀H₃₀N₂O₃S₂
Molecular Weight:410.602
Hs Code.:

Synonyms:5-<3,5-bis(1,1-dimethylethyl)-4-<(2-methoxyethoxy)methoxy>phenyl>-1,3,4-thiadiazole-2(3H)-thione

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Chemical Property of 5-<3,5-bis(1,1-dimethylethyl)-4-<(2-methoxyethoxy)methoxy>phenyl>-1,3,4-thiadiazole-2(3H)-thione

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Technology Process of 5-<3,5-bis(1,1-dimethylethyl)-4-<(2-methoxyethoxy)methoxy>phenyl>-1,3,4-thiadiazole-2(3H)-thione

There total 3 articles about 5-<3,5-bis(1,1-dimethylethyl)-4-<(2-methoxyethoxy)methoxy>phenyl>-1,3,4-thiadiazole-2(3H)-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 75-15-0,12122-00-8
carbon disulfide

: 130116-74-4
3,5-bis(1,1-dimethylethyl)-4-<(2-methoxyethoxy)methoxy>benzenecarboximidic acid hydrazide

: 130116-75-5
5-<3,5-bis(1,1-dimethylethyl)-4-<(2-methoxyethoxy)methoxy>phenyl>-1,3,4-thiadiazole-2(3H)-thione

Guidance literature:: In ethanol; for 3h; Ambient temperature;
DOI:10.1021/jm00060a017

Reference yield:

: 1988-88-1
2,6-di-tert-butyl-4-cyanophenol

: 130116-75-5
5-<3,5-bis(1,1-dimethylethyl)-4-<(2-methoxyethoxy)methoxy>phenyl>-1,3,4-thiadiazole-2(3H)-thione

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / diisopropylaminomethane / CH₂Cl₂ / 18 h / Ambient temperature

2: 1.) NaH, 97percent hydrazine / 1.) THF, 0 deg C, 1.5 h, 2.) THF, 0 deg C, 2 h

3: 80 percent / ethanol / 3 h / Ambient temperature

With N,N-diisopropylmethylamine; sodium hydride; hydrazine hydrate; In ethanol; dichloromethane;
DOI:10.1021/jm00060a017

Reference yield:

: 130116-73-3
3,5-bis(1,1-dimethylethyl)-4-<(2-methoxyethoxy)methoxy>benzonitrile

: 130116-75-5
5-<3,5-bis(1,1-dimethylethyl)-4-<(2-methoxyethoxy)methoxy>phenyl>-1,3,4-thiadiazole-2(3H)-thione

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH, 97percent hydrazine / 1.) THF, 0 deg C, 1.5 h, 2.) THF, 0 deg C, 2 h

2: 80 percent / ethanol / 3 h / Ambient temperature

With sodium hydride; hydrazine hydrate; In ethanol;
DOI:10.1021/jm00060a017