Ethoxycarbonylmethyl-benzyl-disulfid

Base Information

Chemical Name:Ethoxycarbonylmethyl-benzyl-disulfid
CAS No.:21230-19-3
Molecular Formula:C₁₁H₁₄O₂S₂
Molecular Weight:242.363
Hs Code.:

Synonyms:Ethoxycarbonylmethyl-benzyl-disulfid

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Chemical Property of Ethoxycarbonylmethyl-benzyl-disulfid

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Technology Process of Ethoxycarbonylmethyl-benzyl-disulfid

There total 6 articles about Ethoxycarbonylmethyl-benzyl-disulfid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 104340-32-1
(benzimidazol-2-yl) benzyl sulfoxide

: 623-51-8
ethyl 2-sulfanylacetate

: 5429-62-9
ethyl 2-(1H-benzo[d]imidazol-2-ylthio)acetate

: 21230-19-3
Ethoxycarbonylmethyl-benzyl-disulfid

Guidance literature:: In ethanol; at 25 ℃;
DOI:10.1021/jo00229a039

Reference yield:

: 51290-77-8
2-(benzylthio)-1H-benzo[d]imidazole

: 21230-19-3
Ethoxycarbonylmethyl-benzyl-disulfid

Guidance literature:: Multi-step reaction with 2 steps

1: m-chloroperbenzoic acid / CHCl₃ / 0.17 h / 0 - 5 °C

2: 75 percent / aq. ethanol / 25 °C

With 3-chloro-benzenecarboperoxoic acid; In ethanol; chloroform;
DOI:10.1021/jo00229a039

Reference yield:

: 100-44-7
benzyl chloride

: 21230-19-3
Ethoxycarbonylmethyl-benzyl-disulfid

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / ethanol; H₂O / 2.5 h / Heating

2: m-chloroperbenzoic acid / CHCl₃ / 0.17 h / 0 - 5 °C

3: 75 percent / aq. ethanol / 25 °C

With sodium hydroxide; 3-chloro-benzenecarboperoxoic acid; In ethanol; chloroform; water;
DOI:10.1021/jo00229a039