(2S,8S)-2-(tert-butyldiphenylsilanyloxymethyl)-8-methanesulphonyloxymethyl-3,4,6,7,8,9,-hexahydro-2H-pyrimido[1,2-a]pyrimidin-1-ium hexafluorophosphate

Base Information

Chemical Name:(2S,8S)-2-(tert-butyldiphenylsilanyloxymethyl)-8-methanesulphonyloxymethyl-3,4,6,7,8,9,-hexahydro-2H-pyrimido[1,2-a]pyrimidin-1-ium hexafluorophosphate
CAS No.:577750-51-7
Molecular Formula:C₂₆H₃₇N₃O₄SSi*F₆P*H
Molecular Weight:661.721
Hs Code.:

(2S,8S)-2-(tert-butyldiphenylsilanyloxymethyl)-8-methanesulphonyloxymethyl-3,4,6,7,8,9,-hexahydro-2H-pyrimido[1,2-a]pyrimidin-1-ium hexafluorophosphate

Synonyms:(2S,8S)-2-(tert-butyldiphenylsilanyloxymethyl)-8-methanesulphonyloxymethyl-3,4,6,7,8,9,-hexahydro-2H-pyrimido[1,2-a]pyrimidin-1-ium hexafluorophosphate

Suppliers and Price of (2S,8S)-2-(tert-butyldiphenylsilanyloxymethyl)-8-methanesulphonyloxymethyl-3,4,6,7,8,9,-hexahydro-2H-pyrimido[1,2-a]pyrimidin-1-ium hexafluorophosphate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S,8S)-2-(tert-butyldiphenylsilanyloxymethyl)-8-methanesulphonyloxymethyl-3,4,6,7,8,9,-hexahydro-2H-pyrimido[1,2-a]pyrimidin-1-ium hexafluorophosphate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S,8S)-2-(tert-butyldiphenylsilanyloxymethyl)-8-methanesulphonyloxymethyl-3,4,6,7,8,9,-hexahydro-2H-pyrimido[1,2-a]pyrimidin-1-ium hexafluorophosphate

There total 1 articles about (2S,8S)-2-(tert-butyldiphenylsilanyloxymethyl)-8-methanesulphonyloxymethyl-3,4,6,7,8,9,-hexahydro-2H-pyrimido[1,2-a]pyrimidin-1-ium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 577750-36-8
C₂₅H₃₅N₃O₂Si*F₆P^(1-)*H⁽¹⁺⁾

: 7143-01-3
Methanesulfonic anhydride

: 577750-51-7
(2S,8S)-2-(tert-butyldiphenylsilanyloxymethyl)-8-methanesulphonyloxymethyl-3,4,6,7,8,9,-hexahydro-2H-pyrimido[1,2-a]pyrimidin-1-ium hexafluorophosphate

Guidance literature:: C₂₅H₃₅N₃O₂Si*F₆P^(1-)*H⁽¹⁺⁾; Methanesulfonic anhydride; With 4-methyl-morpholine; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere;

With ammonium hexafluorophosphate; In dichloromethane; Inert atmosphere;
DOI:10.1080/10610278.2013.835814

Reference yield: 88.0%

: C₂₇H₃₇N₃O₂SSi*F₆P^(1-)*H⁽¹⁺⁾

: 577750-51-7
(2S,8S)-2-(tert-butyldiphenylsilanyloxymethyl)-8-methanesulphonyloxymethyl-3,4,6,7,8,9,-hexahydro-2H-pyrimido[1,2-a]pyrimidin-1-ium hexafluorophosphate

: (2S,8S)-2-(tert-butyldiphenylsilanyloxymethyl)-8-[(2R,8R)-8-(tert-butyldiphenylsilanyloxymethyl)-3,4,6,7,8,9-hexahydro-2H-pyrimido[1,2-a]pyrimidin-2-ylmethylsulphanylmethyl-1-ium hexafluorophosphate]-3,4,6,7,8,9-hexahydro-2H-pyrimido[1,2-a]pyrimidin-1-ium hexafluorophosphate

Guidance literature:: C₂₇H₃₇N₃O₂SSi*F₆P^(1-)*H⁽¹⁺⁾; (2S,8S)-2-(tert-butyldiphenylsilanyloxymethyl)-8-methanesulphonyloxymethyl-3,4,6,7,8,9,-hexahydro-2H-pyrimido[1,2-a]pyrimidin-1-ium hexafluorophosphate; With caesium carbonate; In methanol; acetonitrile; at 0 ℃; for 4h; Inert atmosphere;

With ammonium hexafluorophosphate; In dichloromethane; water; Inert atmosphere;
DOI:10.1080/10610278.2013.835814