2-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-5-(1-phenyl-1,2,3-triazol-4-yl)-1,3,4-oxadiazole

Base Information

Chemical Name:2-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-5-(1-phenyl-1,2,3-triazol-4-yl)-1,3,4-oxadiazole
CAS No.:1320161-48-5
Molecular Formula:C₄₄H₃₃N₅O₁₀
Molecular Weight:791.774
Hs Code.:

Synonyms:2-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-5-(1-phenyl-1,2,3-triazol-4-yl)-1,3,4-oxadiazole

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Chemical Property of 2-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-5-(1-phenyl-1,2,3-triazol-4-yl)-1,3,4-oxadiazole

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Technology Process of 2-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-5-(1-phenyl-1,2,3-triazol-4-yl)-1,3,4-oxadiazole

There total 4 articles about 2-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-5-(1-phenyl-1,2,3-triazol-4-yl)-1,3,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1320161-33-8
2-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-5-ethynyl-1,3,4-oxadiazole

: 622-37-7
Phenyl azide

: 1320161-48-5
2-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-5-(1-phenyl-1,2,3-triazol-4-yl)-1,3,4-oxadiazole

Guidance literature:: With copper(II) sulfate; ascorbic acid; In dichloromethane; water; at 50 ℃; for 2h;
DOI:10.1016/j.carres.2011.03.004

Reference yield:

: 706784-62-5
5-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)tetrazole

: 1320161-48-5
2-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-5-(1-phenyl-1,2,3-triazol-4-yl)-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide / toluene / 4 h / Reflux

2: copper(II) sulfate; ascorbic acid / dichloromethane; water / 2 h / 50 °C

With copper(II) sulfate; dicyclohexyl-carbodiimide; ascorbic acid; In dichloromethane; water; toluene;
DOI:10.1016/j.carres.2011.03.004

Reference yield:

: 286369-05-9
2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl cyanide

: 1320161-48-5
2-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-5-(1-phenyl-1,2,3-triazol-4-yl)-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 3 steps

1: azido tributyltin (IV) / diethylene glycol dimethyl ether / 26 h / Reflux

2: dicyclohexyl-carbodiimide / toluene / 4 h / Reflux

3: copper(II) sulfate; ascorbic acid / dichloromethane; water / 2 h / 50 °C

With copper(II) sulfate; dicyclohexyl-carbodiimide; azido tributyltin (IV); ascorbic acid; In dichloromethane; diethylene glycol dimethyl ether; water; toluene;
DOI:10.1016/j.carres.2011.03.004