Technology Process of o-(α-Cyano-ethyl)-phenylisocyanid
There total 5 articles about o-(α-Cyano-ethyl)-phenylisocyanid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine; trichlorophosphate;
In
dichloromethane;
at 0 ℃;
for 2h;
Sealed tube;
DOI:10.1021/acs.orglett.1c02373
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: zinc; ammonium chloride / acetone; water / 20 °C / Sealed tube
2.1: acetic anhydride / 2 h / 55 °C / Sealed tube
2.2: 2 h / 0 - 25 °C / Sealed tube
3.1: triethylamine; trichlorophosphate / dichloromethane / 2 h / 0 °C / Sealed tube
With
acetic anhydride; ammonium chloride; triethylamine; zinc; trichlorophosphate;
In
dichloromethane; water; acetone;
DOI:10.1021/acs.orglett.1c02373
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: acetic anhydride / 2 h / 55 °C / Sealed tube
1.2: 2 h / 0 - 25 °C / Sealed tube
2.1: triethylamine; trichlorophosphate / dichloromethane / 2 h / 0 °C / Sealed tube
With
acetic anhydride; triethylamine; trichlorophosphate;
In
dichloromethane;
DOI:10.1021/acs.orglett.1c02373
