(1,5-cyclooctadiene)chloro{bis{bis(trimethylsilyl)methyl}chlorophosphine}rhodium(I)

Base Information

Chemical Name:(1,5-cyclooctadiene)chloro{bis{bis(trimethylsilyl)methyl}chlorophosphine}rhodium(I)
CAS No.:89178-74-5
Molecular Formula:C₂₂H₅₀Cl₂PRhSi₄
Molecular Weight:631.766
Hs Code.:

Synonyms:(1,5-cyclooctadiene)chloro{bis{bis(trimethylsilyl)methyl}chlorophosphine}rhodium(I)

Suppliers and Price of (1,5-cyclooctadiene)chloro{bis{bis(trimethylsilyl)methyl}chlorophosphine}rhodium(I)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1,5-cyclooctadiene)chloro{bis{bis(trimethylsilyl)methyl}chlorophosphine}rhodium(I)

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Technology Process of (1,5-cyclooctadiene)chloro{bis{bis(trimethylsilyl)methyl}chlorophosphine}rhodium(I)

There total 4 articles about (1,5-cyclooctadiene)chloro{bis{bis(trimethylsilyl)methyl}chlorophosphine}rhodium(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 12092-47-6
di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

: 63429-87-8
bischlorophosphorus

: 108-88-3,15644-74-3,16713-13-6
toluene

: 89178-74-5
(1,5-cyclooctadiene)chloro{bis{bis(trimethylsilyl)methyl}chlorophosphine}rhodium(I)-toluene

Guidance literature:: In toluene; phosphine was added to a toluene soln. of (RhCl(COD))2 at 25°C under inert atmosphere, mixt. was stirred for 12 h; volatiles were removed in vacuo, toluene and hexane were added, mixt. was filtered though a Celite pad, concd., filtered again, filtrate cooled to -20°C, crystn.;