1,2-di-tert-butyl 3-phenyl-1H,2H,3H,10bH-[1,2,3,4]tetrazolo[5,1-a]isoquinoline-1,2-dicarboxylate

Base Information

Chemical Name:1,2-di-tert-butyl 3-phenyl-1H,2H,3H,10bH-[1,2,3,4]tetrazolo[5,1-a]isoquinoline-1,2-dicarboxylate
CAS No.:203586-15-6
Molecular Formula:C₂₅H₃₀N₄O₄
Molecular Weight:450.538
Hs Code.:

Synonyms:1,2-di-tert-butyl 3-phenyl-1H,2H,3H,10bH-[1,2,3,4]tetrazolo[5,1-a]isoquinoline-1,2-dicarboxylate

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Chemical Property of 1,2-di-tert-butyl 3-phenyl-1H,2H,3H,10bH-[1,2,3,4]tetrazolo[5,1-a]isoquinoline-1,2-dicarboxylate

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Technology Process of 1,2-di-tert-butyl 3-phenyl-1H,2H,3H,10bH-[1,2,3,4]tetrazolo[5,1-a]isoquinoline-1,2-dicarboxylate

There total 7 articles about 1,2-di-tert-butyl 3-phenyl-1H,2H,3H,10bH-[1,2,3,4]tetrazolo[5,1-a]isoquinoline-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31382-99-7
2-Anilino-isochinolinium-betain

: 870-50-8
di-tert-butyl-diazodicarboxylate

: 203586-15-6
1,2-di-tert-butyl 3-phenyl-1H,2H,3H,10bH-[1,2,3,4]tetrazolo[5,1-a]isoquinoline-1,2-dicarboxylate

Guidance literature:: With carbon disulfide;
DOI:10.1107/S2053229619010210

Reference yield:

: 2-Phenylamino-isoquinolinium; chloride

: 203586-15-6
1,2-di-tert-butyl 3-phenyl-1H,2H,3H,10bH-[1,2,3,4]tetrazolo[5,1-a]isoquinoline-1,2-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Na₂CO₃ / 1.) H₂O

2: CH₂Cl₂

With sodium carbonate; In dichloromethane;
DOI:10.1002/(SICI)1099-0690(199802)1998:2<379::AID-EJOC379>3.0.CO;2-F

Reference yield:

: 33107-14-1
2-(2,4-dinitrophenyl)-isoquinolinium chloride

: 203586-15-6
1,2-di-tert-butyl 3-phenyl-1H,2H,3H,10bH-[1,2,3,4]tetrazolo[5,1-a]isoquinoline-1,2-dicarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 73 percent / triethylamine / ethanol / Ambient temperature

2: 91 percent / conc. HCl / methanol; H₂O / Heating

3: 1.) Na₂CO₃ / 1.) H₂O

4: CH₂Cl₂

With hydrogenchloride; sodium carbonate; triethylamine; In methanol; ethanol; dichloromethane; water;
DOI:10.1002/(SICI)1099-0690(199802)1998:2<379::AID-EJOC379>3.0.CO;2-F