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Technology Process of (Fe[H25C12OC6H4C(O)OC6H3(O)CHNCH2CH2NHC2H5]2)(1+)*PF6(1-)=Fe[H25C12OC6H4C(O)OC6H3(O)CHNCH2CH2NHC2H5]2PF6

(Fe[H25C12OC6H4C(O)OC6H3(O)CHNCH2CH2NHC2H5]2)(1+)*PF6(1-)=Fe[H25C12OC6H4C(O)OC6H3(O)CHNCH2CH2NHC2H5]2PF6

Base Information
  • Chemical Name:(Fe[H25C12OC6H4C(O)OC6H3(O)CHNCH2CH2NHC2H5]2)(1+)*PF6(1-)=Fe[H25C12OC6H4C(O)OC6H3(O)CHNCH2CH2NHC2H5]2PF6
  • CAS No.:399566-84-8
  • Molecular Formula:C60H86FeN4O8*F6P
  • Molecular Weight:1192.18
  • Hs Code.:
(Fe[H<sub>25</sub>C<sub>12</sub>OC<sub>6</sub>H<sub>4</sub>C(O)OC<sub>6</sub>H<sub>3</sub>(O)CHNCH<sub>2</sub>CH<sub>2</sub>NHC<sub>2</sub>H<sub>5</sub>]2)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=Fe[H<sub>25</sub>C<sub>12</sub>OC<sub>6</sub>H<sub>4</sub>C(O)OC<sub>6</sub>H<sub>3</sub>(O)CHNCH<sub>2</sub>CH<sub>2</sub>NHC<sub>2</sub>H<sub>5</sub>]2PF<sub>6</sub>

Synonyms:(Fe[H25C12OC6H4C(O)OC6H3(O)CHNCH2CH2NHC2H5]2)(1+)*PF6(1-)=Fe[H25C12OC6H4C(O)OC6H3(O)CHNCH2CH2NHC2H5]2PF6

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Chemical Property of (Fe[H25C12OC6H4C(O)OC6H3(O)CHNCH2CH2NHC2H5]2)(1+)*PF6(1-)=Fe[H25C12OC6H4C(O)OC6H3(O)CHNCH2CH2NHC2H5]2PF6
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Technology Process of (Fe[H25C12OC6H4C(O)OC6H3(O)CHNCH2CH2NHC2H5]2)(1+)*PF6(1-)=Fe[H25C12OC6H4C(O)OC6H3(O)CHNCH2CH2NHC2H5]2PF6

There total 1 articles about (Fe[H25C12OC6H4C(O)OC6H3(O)CHNCH2CH2NHC2H5]2)(1+)*PF6(1-)=Fe[H25C12OC6H4C(O)OC6H3(O)CHNCH2CH2NHC2H5]2PF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

potassium hexafluorophosphate
17084-13-8

potassium hexafluorophosphate

N-ethylethane-1,2-diamine
110-72-5

N-ethylethane-1,2-diamine

Iron(III) nitrate nonahydrate

Iron(III) nitrate nonahydrate

4-(2`hydroxy-4`-dodecylhydroxybenzoylhydroxy)benzaldehyde
868620-29-5

4-(2`hydroxy-4`-dodecylhydroxybenzoylhydroxy)benzaldehyde

(Fe[H<sub>25</sub>C<sub>12</sub>OC<sub>6</sub>H<sub>4</sub>C(O)OC<sub>6</sub>H<sub>3</sub>(O)CHNCH<sub>2</sub>CH<sub>2</sub>NHC<sub>2</sub>H<sub>5</sub>]2)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=Fe[H<sub>25</sub>C<sub>12</sub>OC<sub>6</sub>H<sub>4</sub>C(O)OC<sub>6</sub>H<sub>3</sub>(O)CHNCH<sub>2</sub>CH<sub>2</sub>NHC<sub>2</sub>H<sub>5</sub>]2PF<sub>6</sub>
399566-84-8

(Fe[H25C12OC6H4C(O)OC6H3(O)CHNCH2CH2NHC2H5]2)(1+)*PF6(1-)=Fe[H25C12OC6H4C(O)OC6H3(O)CHNCH2CH2NHC2H5]2PF6

Guidance literature:
With NaOH; In ethanol; water; the amine added in small protions to the aldehyde in C2H5OH; heated for 20 min at 100°C; aq. NaOH added; Fe(NO3)3*9H2O in C2H5OH added with stirring; excess of KPF6 added to suspn.; heated at reflux for 15 min; ppt. filtered from hot soln.; ppt. washed with CH3OH and dried in vacuo;elem. anal.;
DOI:10.1002/1521-3773(20011119)40:22<4269::AID-ANIE4269>3.0.CO;2-8
upstream raw materials:

potassium hexafluorophosphate

N-ethylethane-1,2-diamine

4-(2`hydroxy-4`-dodecylhydroxybenzoylhydroxy)benzaldehyde

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