ethyl 16-amino-7,14-bis[(4-methylphenyl)sulfonyl]-3-tridecyl-4,7,14-triazahexadecanoate

Base Information

Chemical Name:ethyl 16-amino-7,14-bis[(4-methylphenyl)sulfonyl]-3-tridecyl-4,7,14-triazahexadecanoate
CAS No.:544696-92-6
Molecular Formula:C₄₂H₇₂N₄O₆S₂
Molecular Weight:793.189
Hs Code.:

Synonyms:ethyl 16-amino-7,14-bis[(4-methylphenyl)sulfonyl]-3-tridecyl-4,7,14-triazahexadecanoate

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Chemical Property of ethyl 16-amino-7,14-bis[(4-methylphenyl)sulfonyl]-3-tridecyl-4,7,14-triazahexadecanoate

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Technology Process of ethyl 16-amino-7,14-bis[(4-methylphenyl)sulfonyl]-3-tridecyl-4,7,14-triazahexadecanoate

There total 9 articles about ethyl 16-amino-7,14-bis[(4-methylphenyl)sulfonyl]-3-tridecyl-4,7,14-triazahexadecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: ethyl 3-{{2-{{6-{(2-aminoethyl)[(4-methylphenyl)sulfonyl]amino}hexyl}[(4-methylphenyl)sulfonyl]amino}ethyl}amino}hexadec-2-enoate

: 544696-92-6
ethyl 16-amino-7,14-bis[(4-methylphenyl)sulfonyl]-3-tridecyl-4,7,14-triazahexadecanoate

Guidance literature:: With hydrogen; platinum(IV) oxide; In ethanol; chloroform; at 20 ℃; for 4h; under 2844.31 Torr;
DOI:10.1002/hlca.200390033

Reference yield:

: 124-09-4
1,6-Hexanediamine

: 544696-92-6
ethyl 16-amino-7,14-bis[(4-methylphenyl)sulfonyl]-3-tridecyl-4,7,14-triazahexadecanoate

Guidance literature:: Multi-step reaction with 5 steps

1: 71 percent / KF/Celite / acetonitrile / 48 h / 20 °C

2: 90 percent / Et₃N / CH₂Cl₂ / 12 h / 20 °C

3: 95 percent / H₂; NH₄OH / Raney-Ni / ethanol; H₂O / 20 h / 20 °C / 2844.31 Torr

4: 63 percent / ethanol / 2 h / Heating

5: 90 percent / H₂ / PtO₂ / CHCl₃; ethanol / 4 h / 20 °C / 2844.31 Torr

With ammonium hydroxide; hydrogen; triethylamine; platinum(IV) oxide; potassium fluoride; Celite; nickel; In ethanol; dichloromethane; chloroform; water; acetonitrile; 4: Michael addition;
DOI:10.1002/hlca.200390033

Reference yield:

: 765-09-3
1-bromotridecane

: 544696-92-6
ethyl 16-amino-7,14-bis[(4-methylphenyl)sulfonyl]-3-tridecyl-4,7,14-triazahexadecanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / dimethylsulfoxide / 1 h / 20 °C

2: 85 percent / BuLi / hexane; tetrahydrofuran / 1 h / 0 °C

3: 63 percent / ethanol / 2 h / Heating

4: 90 percent / H₂ / PtO₂ / CHCl₃; ethanol / 4 h / 20 °C / 2844.31 Torr

With n-butyllithium; hydrogen; platinum(IV) oxide; In tetrahydrofuran; ethanol; hexane; chloroform; dimethyl sulfoxide; 3: Michael addition;
DOI:10.1002/hlca.200390033