α-acetoxy-1-(allyloxycarbonyl)-2,2-dibenzylhydrazineacetic acid methyl ester

Base Information

Chemical Name:α-acetoxy-1-(allyloxycarbonyl)-2,2-dibenzylhydrazineacetic acid methyl ester
CAS No.:155219-96-8
Molecular Formula:C₂₃H₂₆N₂O₆
Molecular Weight:426.469
Hs Code.:

Synonyms:α-acetoxy-1-(allyloxycarbonyl)-2,2-dibenzylhydrazineacetic acid methyl ester

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Chemical Property of α-acetoxy-1-(allyloxycarbonyl)-2,2-dibenzylhydrazineacetic acid methyl ester

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Technology Process of α-acetoxy-1-(allyloxycarbonyl)-2,2-dibenzylhydrazineacetic acid methyl ester

There total 3 articles about α-acetoxy-1-(allyloxycarbonyl)-2,2-dibenzylhydrazineacetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-44-7
benzyl chloride

: 155219-96-8
α-acetoxy-1-(allyloxycarbonyl)-2,2-dibenzylhydrazineacetic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / K₂CO₃, LiI / ethanol / 18 h / Heating

2: toluene / 40 h

3: pyridine / DMAP / 18 h / Ambient temperature

With pyridine; potassium carbonate; lithium iodide; dmap; In ethanol; toluene;
DOI:10.1016/S0040-4020(01)96267-2

Reference yield:

: 155219-85-5
1,1-dibenzyl-2-hydrazinecarboxylic acid allyl ester

: 155219-96-8
α-acetoxy-1-(allyloxycarbonyl)-2,2-dibenzylhydrazineacetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 40 h

2: pyridine / DMAP / 18 h / Ambient temperature

With pyridine; dmap; In toluene;
DOI:10.1016/S0040-4020(01)96267-2