4-((4-((2-(tert-butoxycarbonylamino)acetamido)methyl)phenyl)diazenyl)benzoic acid

Base Information

Chemical Name:4-((4-((2-(tert-butoxycarbonylamino)acetamido)methyl)phenyl)diazenyl)benzoic acid
CAS No.:915088-40-3
Molecular Formula:C₂₁H₂₄N₄O₅
Molecular Weight:412.445
Hs Code.:

Synonyms:4-((4-((2-(tert-butoxycarbonylamino)acetamido)methyl)phenyl)diazenyl)benzoic acid

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Chemical Property of 4-((4-((2-(tert-butoxycarbonylamino)acetamido)methyl)phenyl)diazenyl)benzoic acid

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Technology Process of 4-((4-((2-(tert-butoxycarbonylamino)acetamido)methyl)phenyl)diazenyl)benzoic acid

There total 1 articles about 4-((4-((2-(tert-butoxycarbonylamino)acetamido)methyl)phenyl)diazenyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 915088-38-9
ethyl 4-((4-((2-(tert-butoxycarbonylamino)acetamido)methyl)phenyl)diazenyl)benzoate

: 915088-40-3
4-((4-((2-(tert-butoxycarbonylamino)acetamido)methyl)phenyl)diazenyl)benzoic acid

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; water; at 50 ℃; for 16h;
DOI:10.1039/b609320p

Reference yield: 69.0%

: 915088-40-3
4-((4-((2-(tert-butoxycarbonylamino)acetamido)methyl)phenyl)diazenyl)benzoic acid

: 139163-87-4
(2R,3S)-methyl 3-amino-2-hydroxy-4-phenylbutanoate

: 1240365-14-3
(2R,3S,E)-methyl 3-(4-((4-((2-(tert-butoxycarbonylamino) acetamido)methyl)phenyl)diazenyl)benzamido)-2-hydroxy-4-phenylbutanoate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 16h;
DOI:10.1002/chem.200903369

Reference yield: 60.0%

: 915088-40-3
4-((4-((2-(tert-butoxycarbonylamino)acetamido)methyl)phenyl)diazenyl)benzoic acid

: 94242-84-9
4,4,5,5-tetramethyl-α-(phenylmethyl)-1,3,2-dioxaborolane-2-methanamine, trifluoroacetic acid salt

: 915088-24-3
(CH₃)3COC(O)NHCH₂C(O)NHCH₂C₆H₄NNC₆H₄C(O)NHCH(CH₂C₆H₅)BOC(CH₃)2C(CH₃)2O

Guidance literature:: With 4-methyl-morpholine; isobutyl chloroformate; In N,N-dimethyl-formamide; isobutylchloroformate and NMM added to cooled (ice bath) soln. of substituted benzoic acid in DMF; stirred for 10 min; soln. of B compd. in DMF added; stirred for 16 h; warmed from 0°C to room temp.; diluted with ethyl acetate; washed with H2O, brine; dried (MgSO4); filtered; concd.; purifed by column chromy. (deactivated silica, EtOAc);
DOI:10.1039/b609320p