(E)-N-cyclohexyl-1-(thiophen-2-yl)methanimine

Base Information

Chemical Name:(E)-N-cyclohexyl-1-(thiophen-2-yl)methanimine
CAS No.:926312-67-6
Molecular Formula:C₁₁H₁₅NS
Molecular Weight:193.313
Hs Code.:

Synonyms:(E)-N-cyclohexyl-1-(thiophen-2-yl)methanimine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-cyclohexyl-1-(thiophen-2-yl)methanimine

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Technology Process of (E)-N-cyclohexyl-1-(thiophen-2-yl)methanimine

There total 1 articles about (E)-N-cyclohexyl-1-(thiophen-2-yl)methanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 10354-42-4
N-cyclohexylthiophene-2-carboxamide

: 926312-67-6
(E)-N-cyclohexyl-1-(thiophen-2-yl)methanimine

Guidance literature:: N-cyclohexylthiophene-2-carboxamide; With 2-fluoropyridine; trifluoromethylsulfonic anhydride; In dichloromethane; at -78 - 0 ℃; Inert atmosphere;

With triethylsilane; In dichloromethane; at 0 - 25 ℃; Inert atmosphere;

With sodium hydrogencarbonate; In dichloromethane; water; chemoselective reaction;
DOI:10.1021/ja105194s

Reference yield: 62.0%

: 926312-67-6
(E)-N-cyclohexyl-1-(thiophen-2-yl)methanimine

: 3375-31-3
palladium diacetate

: 1015807-40-5
[palladium(II)(5-SC₄H₂C(H)=NCy)(O₂CMe)]2

Guidance literature:: In toluene; (Ar); organic ligand and Pd(OAc)2 added to dry toluene; soln. heated at 80°C for 3 h; cooled to room temp.; filtered; solvent removed under vacuum; chromatographed on silica gel column; eluted with CH2Cl2/CH3OH (1%); concd.; recrystallized from CHCl3/hexane; elem. anal.;
DOI:10.1002/zaac.200600371

Reference yield: 52.0%

: 15321-51-4
diiron nonacarbonyl

: 926312-67-6
(E)-N-cyclohexyl-1-(thiophen-2-yl)methanimine

: Fe2(CO)6(μ2-η(3)-C6H11NCH2C=CCH=CHS)

Guidance literature:: In n-heptane; Ar-atmosphere; stirring Fe-complex with 1.5 equiv. of imine to dissoln. at 50°C; solvent removal (vac.), dissoln. in CH2Cl2, addn. of silanized silica gel, solvent removal, chromy. (petroleum ether); elem. anal.; further unidentified product;
DOI:10.1016/S0022-328X(96)06824-6