3-(2-(2-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethoxy)ethoxy)ethoxy)benzyl azide

Base Information

Chemical Name:3-(2-(2-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethoxy)ethoxy)ethoxy)benzyl azide
CAS No.:1440529-29-2
Molecular Formula:C₂₀H₃₃N₃O₇
Molecular Weight:427.498
Hs Code.:

Synonyms:3-(2-(2-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethoxy)ethoxy)ethoxy)benzyl azide

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Chemical Property of 3-(2-(2-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethoxy)ethoxy)ethoxy)benzyl azide

Chemical Property:

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Technology Process of 3-(2-(2-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethoxy)ethoxy)ethoxy)benzyl azide

There total 4 articles about 3-(2-(2-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethoxy)ethoxy)ethoxy)benzyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1440529-36-1
3-(2-(2-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethoxy)ethoxy)ethoxy)benzyl bromide

: 1440529-29-2
3-(2-(2-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethoxy)ethoxy)ethoxy)benzyl azide

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 60 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.bmc.2013.02.045

Reference yield:

: 1440529-35-0
3-(2-(2-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethoxy)ethoxy)ethoxy)benzyl alcohol

: 1440529-29-2
3-(2-(2-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethoxy)ethoxy)ethoxy)benzyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus tribromide / diethyl ether / 20 h / 0 - 20 °C / Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 24 h / 60 °C / Inert atmosphere

With sodium azide; phosphorus tribromide; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2013.02.045

Reference yield:

: 155887-96-0,58320-73-3
2,5,8,11,14,17-hexaoxanonadecan-19-yl 4-methylbenzenesulfonate

: 1440529-29-2
3-(2-(2-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethoxy)ethoxy)ethoxy)benzyl azide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 48 h / Reflux

2: phosphorus tribromide / diethyl ether / 20 h / 0 - 20 °C / Inert atmosphere

3: sodium azide / N,N-dimethyl-formamide / 24 h / 60 °C / Inert atmosphere

With sodium azide; phosphorus tribromide; potassium carbonate; In diethyl ether; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmc.2013.02.045