tert-butyl 4-((tert-butyldimethylsilyloxy)methyl)-2-methoxyphenylcarbamate

Base Information

Chemical Name:tert-butyl 4-((tert-butyldimethylsilyloxy)methyl)-2-methoxyphenylcarbamate
CAS No.:882430-28-6
Molecular Formula:C₁₉H₃₃NO₄Si
Molecular Weight:367.561
Hs Code.:

Synonyms:tert-butyl 4-((tert-butyldimethylsilyloxy)methyl)-2-methoxyphenylcarbamate

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Chemical Property of tert-butyl 4-((tert-butyldimethylsilyloxy)methyl)-2-methoxyphenylcarbamate

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Technology Process of tert-butyl 4-((tert-butyldimethylsilyloxy)methyl)-2-methoxyphenylcarbamate

There total 5 articles about tert-butyl 4-((tert-butyldimethylsilyloxy)methyl)-2-methoxyphenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 882430-23-1
4-((tert-butyldimethylsilyloxy)methyl)-2-methoxyaniline

: 882430-28-6
tert-butyl 4-((tert-butyldimethylsilyloxy)methyl)-2-methoxyphenylcarbamate

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; water; at 20 ℃;

Reference yield:

: 80866-88-2
(3-methoxy-4-nitrophenyl)methanol

: 882430-28-6
tert-butyl 4-((tert-butyldimethylsilyloxy)methyl)-2-methoxyphenylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / imidazole / dimethylformamide

2: 98 percent / H₂ / Pd/C / methanol

3: 92 percent / tetrahydrofuran

With 1H-imidazole; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2005.06.006

Reference yield:

: 882430-21-9
tert-butyl(3-methoxy-4-nitrobenzyloxy)dimethylsilane

: 882430-28-6
tert-butyl 4-((tert-butyldimethylsilyloxy)methyl)-2-methoxyphenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / H₂ / Pd/C / methanol

2: 92 percent / tetrahydrofuran

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2005.06.006