4-Fluoro-4'-nitrodiphenylamine

Base Information

Chemical Name:4-Fluoro-4'-nitrodiphenylamine
CAS No.:330-89-2
Molecular Formula:C12H9 F N2 O2
Molecular Weight:232.21
Hs Code.:2921420090
Mol file:330-89-2.mol

Synonyms:4-Fluoro-4'-nitrodiphenylamine

Suppliers and Price of 4-Fluoro-4'-nitrodiphenylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4-FLUORO-4'-NITRODIPHENYLAMINE 95.00%
5MG
$ 497.84

Total 7 raw suppliers

Chemical Property of 4-Fluoro-4'-nitrodiphenylamine

Chemical Property:

PSA：57.85000
LogP:4.07370

Purity/Quality:

98%min ^*data from raw suppliers

4-FLUORO-4'-NITRODIPHENYLAMINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-Fluoro-4'-nitrodiphenylamine

There total 6 articles about 4-Fluoro-4'-nitrodiphenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 352-34-1
4-fluoro-1-iodobenzene

: 100-01-6,104810-17-5
4-nitro-aniline

: 330-89-2
4-fluoro-N-(4-nitrophenyl)aniline

Guidance literature:: With silver hexafluoroantimonate; chloro[di(1-adamantyl)-2-dimethylaminophenylphosphine]gold(I); In methanol; at 0 - 80 ℃; Inert atmosphere;
DOI:10.1021/acs.orglett.9b03082

Reference yield: 50.0%

: N-(4-fluorophenyl)-4-nitrobenzenesulfinamide

: 330-89-2
4-fluoro-N-(4-nitrophenyl)aniline

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 16h; Inert atmosphere;
DOI:10.1021/acs.orglett.1c04122

Reference yield:

: 100-32-3
di(p-nitrophenyl) disulfide

: 330-89-2
4-fluoro-N-(4-nitrophenyl)aniline

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide / dichloromethane / 0 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / Inert atmosphere

2.2: -78 °C / Inert atmosphere

3.1: caesium carbonate / N,N-dimethyl-formamide / 16 h / 70 °C / Inert atmosphere

With N-Bromosuccinimide; n-butyllithium; caesium carbonate; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/acs.orglett.1c04122