N-(2,2-diphenylvinyl)-N-phenylamide trichloroacetic acid

Base Information

• Chemical Name: N-(2,2-diphenylvinyl)-N-phenylamide trichloroacetic acid
• CAS No.: 115264-64-7
• Molecular Formula: C₂₂H₁₆Cl₃NO
• Molecular Weight: 416.734

Synonyms:N-(2,2-diphenylvinyl)-N-phenylamide trichloroacetic acid

Chemical Property of N-(2,2-diphenylvinyl)-N-phenylamide trichloroacetic acid

Chemical Property:

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Technology Process of N-(2,2-diphenylvinyl)-N-phenylamide trichloroacetic acid

There total 2 articles about N-(2,2-diphenylvinyl)-N-phenylamide trichloroacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

triphenylketeneimine (14181-84-1) + sodium trichloroacetate (650-51-1) → 2,2-diphenylacetanilide (4695-14-1) + N-(2,2-diphenylvinyl)-N-phenylamide dichloroacetic acid (115264-62-5) + N-(2,2-diphenylvinyl)-N-phenylamide trichloroacetic acid (115264-64-7) + N-(2,2-diphenylvinyl)-N-phenylcarbamoylchloride (108661-30-9)

Guidance literature:

N-benzyl-N,N,N-triethylammonium chloride; In chloroform; at 60 ℃; for 7h; Further byproducts given;

DOI:10.1007/BF00476534

Reference yield: 57.0%

triphenylketeneimine (14181-84-1) + sodium trichloroacetate (650-51-1) → N-(2,2-diphenylvinyl)-N-phenylamide dichloroacetic acid (115264-62-5) + N-(2,2-diphenylvinyl)-N-phenylamide trichloroacetic acid (115264-64-7) + N-(2,2-diphenylvinyl)-N-phenylcarbamoylchloride (108661-30-9) + N-(2,2-diphenylvinyl)-N-(trichlorovinyl)aniline (115264-63-6)

Guidance literature:

N-benzyl-N,N,N-triethylammonium chloride; In chloroform; at 60 ℃; for 7h; Further byproducts given;

DOI:10.1007/BF00476534

Reference yield: 92.0%

N-(2,2-diphenylvinyl)-N-phenylamide trichloroacetic acid (115264-64-7) → N-(2,2-diphenylvinyl)-N-phenylamide dichloroacetic acid (115264-62-5)

Guidance literature:

With sodium trichloroacetate; N-benzyl-N,N,N-triethylammonium chloride; In chloroform; at 60 ℃;

upstream raw materials:

triphenylketeneimine

sodium trichloroacetate

Downstream raw materials:

N-(2,2-diphenylvinyl)-N-phenylamide dichloroacetic acid

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