C₂₇H₃₅N₃OS

Base Information

Chemical Name:C₂₇H₃₅N₃OS
CAS No.:667940-67-2
Molecular Formula:C₂₇H₃₅N₃OS
Molecular Weight:449.66
Hs Code.:

C<sub>27</sub>H<sub>35</sub>N<sub>3</sub>OS

Synonyms:C₂₇H₃₅N₃OS

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₃₅N₃OS

Chemical Property:

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Technology Process of C₂₇H₃₅N₃OS

There total 7 articles about C₂₇H₃₅N₃OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 667940-71-8
C₃₅H₃₇N₃O₃S

: 667940-67-2
C₂₇H₃₅N₃OS

Guidance literature:: With hydrazine; In ethanol;

Reference yield: 57.0%

: 1000819-09-9
C₃₂H₄₃N₃O₃S

: 667940-67-2
C₂₇H₃₅N₃OS

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 0.25h;
DOI:10.1016/j.bmcl.2007.09.099

Reference yield:

: 666852-63-7
ethyl 2-methyl-2-(2-thienyl)propanoate

: 667940-67-2
C₂₇H₃₅N₃OS

Guidance literature:: Multi-step reaction with 8 steps

1.1: nitronium tetrafluoborate / 1,2-dimethoxyethane / 4 h / -55 - -10 °C

2.1: hydrogen / palladium 10% on activated carbon / ethanol; ethyl acetate / 5 h / 1140.08 Torr

3.1: tetrahydrofuran / 16 h / Heating / reflux

4.1: sodium hydroxide; water / ethanol / 1.5 h / Heating / reflux

5.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.17 h

5.2: 20 °C

6.1: sodium hydride / N,N-dimethyl-formamide / 1.5 h

6.2: 5 - 20 °C

7.1: hydrogenchloride / 1,4-dioxane; iso-butanol / 1 h / 90 °C

8.1: hydrazine / ethanol / 16 h / 20 °C

With hydrogenchloride; dmap; sodium hydroxide; nitronium tetrafluoborate; water; hydrogen; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydrazine; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; iso-butanol;