Acenaphthene-5,6-dicarboxylic anhydride

Base Information

Chemical Name:Acenaphthene-5,6-dicarboxylic anhydride
CAS No.:5699-00-3
Molecular Formula:C14H8 O3
Molecular Weight:224.21
Hs Code.:
Mol file:5699-00-3.mol

Synonyms:5,6-Acenaphthenedicarboxylicanhydride (7CI,8CI); Acenaphthalic anhydride

Suppliers and Price of Acenaphthene-5,6-dicarboxylic anhydride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
6,7-Dihydroacenaphtho[5,6-cd]pyran-1,3-dione
250mg
$ 1320.00

TRC
6,7-Dihydroacenaphtho[5,6-cd]pyran-1,3-dione
100mg
$ 670.00

TRC
6,7-Dihydroacenaphtho[5,6-cd]pyran-1,3-dione
10mg
$ 85.00

Total 4 raw suppliers

Chemical Property of Acenaphthene-5,6-dicarboxylic anhydride

Chemical Property:

PSA：43.37000
LogP:2.24900
Solubility.:Chloroform

Purity/Quality:

99% ^*data from raw suppliers

6,7-Dihydroacenaphtho[5,6-cd]pyran-1,3-dione ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses 6,7-Dihydroacenaphtho[5,6-cd]pyran-1,3-dione is an intermediate in synthesizing 3,?5,?6-?Tribromo-?1,?2-?dihydroacenaphthylene (T771875), a derived from Acenaphthene (1,2-Dihydro Acenaphthylene) (D448330), which is a polycyclic aromatic hydrocarbons as carcinogenic agents.

Technology Process of Acenaphthene-5,6-dicarboxylic anhydride

There total 11 articles about Acenaphthene-5,6-dicarboxylic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.7%

: 31458-06-7
N⁵,N⁵,N⁶,N⁶-tetramethyl-1,2-dihydroacenaphthylene-5,6-dicarboxamide

: 5699-00-3
1,2-dihydro-6-oxacyclopentaphenalene-5,7-dione

Guidance literature:: With hydrogenchloride; In water; Reflux;
DOI:10.1002/anie.201210085

Reference yield:

: 5698-99-7
5,6-acenaphthenedicarboxylic acid

: 5699-00-3
1,2-dihydro-6-oxacyclopentaphenalene-5,7-dione

Guidance literature:: In acetic acid; Heating;
DOI:10.1246/bcsj.54.3020

Reference yield:

: 5254-01-3
1,2-diketopyracene

: 5699-00-3
1,2-dihydro-6-oxacyclopentaphenalene-5,7-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / ethanol / 24 h / Heating

2: 60 percent / 0.1 N aq. sodium hydroxide / CH₂Cl₂ / 5 h / Ambient temperature

3: 18.33 h / Irradiation

With sodium hydroxide; In ethanol; dichloromethane;
DOI:10.1021/ja00311a063