trifluoro-methanesulfonic acid 2-(benzyl-{2-[benzyl-(2-trifluoromethanesulfonyloxy-phenyl)-carbamoyl]-cyclohex-1-enecarbonyl}-amino)-phenyl ester

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Chemical Name:trifluoro-methanesulfonic acid 2-(benzyl-{2-[benzyl-(2-trifluoromethanesulfonyloxy-phenyl)-carbamoyl]-cyclohex-1-enecarbonyl}-amino)-phenyl ester
CAS No.:881731-79-9
Molecular Formula:C₃₆H₃₀F₆N₂O₈S₂
Molecular Weight:796.765
Hs Code.:

trifluoro-methanesulfonic acid 2-(benzyl-{2-[benzyl-(2-trifluoromethanesulfonyloxy-phenyl)-carbamoyl]-cyclohex-1-enecarbonyl}-amino)-phenyl ester

Synonyms:trifluoro-methanesulfonic acid 2-(benzyl-{2-[benzyl-(2-trifluoromethanesulfonyloxy-phenyl)-carbamoyl]-cyclohex-1-enecarbonyl}-amino)-phenyl ester

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Chemical Property of trifluoro-methanesulfonic acid 2-(benzyl-{2-[benzyl-(2-trifluoromethanesulfonyloxy-phenyl)-carbamoyl]-cyclohex-1-enecarbonyl}-amino)-phenyl ester

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Technology Process of trifluoro-methanesulfonic acid 2-(benzyl-{2-[benzyl-(2-trifluoromethanesulfonyloxy-phenyl)-carbamoyl]-cyclohex-1-enecarbonyl}-amino)-phenyl ester

There total 2 articles about trifluoro-methanesulfonic acid 2-(benzyl-{2-[benzyl-(2-trifluoromethanesulfonyloxy-phenyl)-carbamoyl]-cyclohex-1-enecarbonyl}-amino)-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 881731-78-8
cyclohexa-1,4-diene-1,2-dicarboxylic acid bis-[benzyl-(2-hydroxy-phenyl)-amide]

: 881731-79-9
trifluoro-methanesulfonic acid 2-(benzyl-{2-[benzyl-(2-trifluoromethanesulfonyloxy-phenyl)-carbamoyl]-cyclohex-1-enecarbonyl}-amino)-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / ethanol; ethyl acetate / 4.5 h

2: 3.88 g / Cs₂CO₃ / dimethylformamide / 1 h

With hydrogen; caesium carbonate; palladium on activated charcoal; In ethanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jo0523363

Reference yield:

: cyclohex-1-ene-1,2-dicarboxylic acid bis-[benzyl-(2-hydroxy-phenyl)-amide]

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 881731-79-9
trifluoro-methanesulfonic acid 2-(benzyl-{2-[benzyl-(2-trifluoromethanesulfonyloxy-phenyl)-carbamoyl]-cyclohex-1-enecarbonyl}-amino)-phenyl ester

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; for 1h;
DOI:10.1021/jo0523363

Reference yield: 64.0%

: 881731-79-9
trifluoro-methanesulfonic acid 2-(benzyl-{2-[benzyl-(2-trifluoromethanesulfonyloxy-phenyl)-carbamoyl]-cyclohex-1-enecarbonyl}-amino)-phenyl ester

: C₃₄H₂₈N₂O₂

: C₃₄H₂₈N₂O₂

Guidance literature:: With triethylamine; bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl acetamide; at 100 ℃; for 24h;
DOI:10.1021/jo0523363