2'-deoxy-6-N-{2-[(1,3-diaza-3-methyl-2-oxophenoxazin-9-yl)oxy]ethyl}-2-(phenoxyacetylamino)adenosine

Base Information

Chemical Name:2'-deoxy-6-N-{2-[(1,3-diaza-3-methyl-2-oxophenoxazin-9-yl)oxy]ethyl}-2-(phenoxyacetylamino)adenosine
CAS No.:1572289-18-9
Molecular Formula:C₃₁H₃₁N₉O₈
Molecular Weight:657.643
Hs Code.:

Synonyms:2'-deoxy-6-N-{2-[(1,3-diaza-3-methyl-2-oxophenoxazin-9-yl)oxy]ethyl}-2-(phenoxyacetylamino)adenosine

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Chemical Property of 2'-deoxy-6-N-{2-[(1,3-diaza-3-methyl-2-oxophenoxazin-9-yl)oxy]ethyl}-2-(phenoxyacetylamino)adenosine

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Technology Process of 2'-deoxy-6-N-{2-[(1,3-diaza-3-methyl-2-oxophenoxazin-9-yl)oxy]ethyl}-2-(phenoxyacetylamino)adenosine

There total 5 articles about 2'-deoxy-6-N-{2-[(1,3-diaza-3-methyl-2-oxophenoxazin-9-yl)oxy]ethyl}-2-(phenoxyacetylamino)adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1609928-35-9
C₄₃H₅₉N₉O₈Si₂

: 1572289-18-9
2'-deoxy-6-N-{2-[(1,3-diaza-3-methyl-2-oxophenoxazin-9-yl)oxy]ethyl}-2-(phenoxyacetylamino)adenosine

Guidance literature:: With triethylamine tris(hydrogen fluoride); In tetrahydrofuran; for 2h;
DOI:10.1016/j.bmc.2014.01.024

Reference yield:

: 328238-59-1
2-amino-9-{(2R,4S,5R)-4-(tert-butyldimethylsilyloxy)-5-[(tert-butyldimethylsilyloxy)methyl]tetrahydrofuran-2-yl}-9H-purine-6-yl 2,4,6-triisopropylbenzenesulfonate

: 1572289-18-9
2'-deoxy-6-N-{2-[(1,3-diaza-3-methyl-2-oxophenoxazin-9-yl)oxy]ethyl}-2-(phenoxyacetylamino)adenosine

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / propan-1-ol / 12 h / 100 °C

2: pyridine / 0 - 20 °C

3: triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 2 h

With pyridine; triethylamine tris(hydrogen fluoride); N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; propan-1-ol;
DOI:10.1016/j.bmc.2014.01.024

Reference yield:

: 961-07-9
2'-Deoxyguanosine

: 1572289-18-9
2'-deoxy-6-N-{2-[(1,3-diaza-3-methyl-2-oxophenoxazin-9-yl)oxy]ethyl}-2-(phenoxyacetylamino)adenosine

Guidance literature:: Multi-step reaction with 5 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 24 h

2: triethylamine; dmap / dichloromethane / 48 h / 20 °C

3: N-ethyl-N,N-diisopropylamine / propan-1-ol / 12 h / 100 °C

4: pyridine / 0 - 20 °C

5: triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 2 h

With pyridine; 1H-imidazole; dmap; triethylamine tris(hydrogen fluoride); triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; propan-1-ol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2014.01.024