1,3,4-tri-O-benzyl-6-O-acetyl-β-D-fructofuranosyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside

Base Information

Chemical Name:1,3,4-tri-O-benzyl-6-O-acetyl-β-D-fructofuranosyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside
CAS No.:1434152-51-8
Molecular Formula:C₅₆H₆₀O₁₂
Molecular Weight:925.085
Hs Code.:

Synonyms:1,3,4-tri-O-benzyl-6-O-acetyl-β-D-fructofuranosyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside

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Chemical Property of 1,3,4-tri-O-benzyl-6-O-acetyl-β-D-fructofuranosyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside

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Technology Process of 1,3,4-tri-O-benzyl-6-O-acetyl-β-D-fructofuranosyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside

There total 4 articles about 1,3,4-tri-O-benzyl-6-O-acetyl-β-D-fructofuranosyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1206803-52-2
6-O-acetyl-1,3,4-tri-O-benzyl-β-D-fructofuranosyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-α-D-glucopyranoside

: 1434152-51-8
1,3,4-tri-O-benzyl-6-O-acetyl-β-D-fructofuranosyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.1016/j.tet.2013.03.094

Reference yield:

: 1206803-49-7
1,3,4-tri-O-benzyl-6-O-triethyl-silyl-β-D-fructofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

: 1434152-51-8
1,3,4-tri-O-benzyl-6-O-acetyl-β-D-fructofuranosyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

2.1: pyridine / 3 h

3.1: dicobalt octacarbonyl; carbon monoxide / 0.33 h / 20 °C

3.2: 70 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

With pyridine; dicobalt octacarbonyl; carbon monoxide; tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1016/j.tet.2013.03.094

Reference yield:

: 1206803-51-1
6-O-acetyl-1,3,4-tri-O-benzyl-β-D-fructofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

: 1434152-51-8
1,3,4-tri-O-benzyl-6-O-acetyl-β-D-fructofuranosyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: dicobalt octacarbonyl; carbon monoxide / 0.33 h / 20 °C

1.2: 70 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

With dicobalt octacarbonyl; carbon monoxide; tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1016/j.tet.2013.03.094