(3aS,7S,7aR)-5-benzyl-7-(hydroxymethyl)-2,2-dimethyl-hexahydro-[1,3]-dioxolo[4,5-c]pyridin-7-ol

Base Information

• Chemical Name: (3aS,7S,7aR)-5-benzyl-7-(hydroxymethyl)-2,2-dimethyl-hexahydro-[1,3]-dioxolo[4,5-c]pyridin-7-ol
• CAS No.: 1052260-22-6
• Molecular Formula: C₁₆H₂₃NO₄
• Molecular Weight: 293.363

Synonyms:(3aS,7S,7aR)-5-benzyl-7-(hydroxymethyl)-2,2-dimethyl-hexahydro-[1,3]-dioxolo[4,5-c]pyridin-7-ol

Chemical Property of (3aS,7S,7aR)-5-benzyl-7-(hydroxymethyl)-2,2-dimethyl-hexahydro-[1,3]-dioxolo[4,5-c]pyridin-7-ol

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Technology Process of (3aS,7S,7aR)-5-benzyl-7-(hydroxymethyl)-2,2-dimethyl-hexahydro-[1,3]-dioxolo[4,5-c]pyridin-7-ol

There total 1 articles about (3aS,7S,7aR)-5-benzyl-7-(hydroxymethyl)-2,2-dimethyl-hexahydro-[1,3]-dioxolo[4,5-c]pyridin-7-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(3aS,7aS)-5-benzyl-2,2-dimethyl-7-methylenehexahydro-[1,3]dioxolo[4,5-c]pyridine (360562-52-3) → (3aS,7S,7aR)-5-benzyl-7-(hydroxymethyl)-2,2-dimethyl-hexahydro-[1,3]-dioxolo[4,5-c]pyridin-7-ol (1052260-22-6)

Guidance literature:

With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; tert-butyl alcohol; at 20 ℃; for 24h;

DOI:10.1039/b804278k

Reference yield: 100.0%

(3aS,7S,7aR)-5-benzyl-7-(hydroxymethyl)-2,2-dimethyl-hexahydro-[1,3]-dioxolo[4,5-c]pyridin-7-ol (1052260-22-6) → (3S,4R,5S)-1-benzyl-3-(hydroxymethyl)piperidine-3,4,5-triol hydrochloride (1052260-25-9)

Guidance literature:

With hydrogenchloride; water; In methanol; at 20 ℃; for 4h;

DOI:10.1039/b804278k

Reference yield: 90.0%

methanesulfonyl chloride (124-63-0) + (3aS,7S,7aR)-5-benzyl-7-(hydroxymethyl)-2,2-dimethyl-hexahydro-[1,3]-dioxolo[4,5-c]pyridin-7-ol (1052260-22-6) → ((3aS,7S,7aR)-5-benzyl-7-hydroxy-2,2-dimethyl-hexahydro-[1,3]dioxolo[4,5-c]pyridin-7-yl)methyl methanesulfonate (1052260-55-5)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1039/b804278k

upstream raw materials:

(3aS,7aS)-5-benzyl-2,2-dimethyl-7-methylenehexahydro-[1,3]dioxolo[4,5-c]pyridine

Downstream raw materials:

((3aS,7S,7aR)-5-benzyl-7-hydroxy-2,2-dimethyl-hexahydro-[1,3]dioxolo[4,5-c]pyridin-7-yl)methyl methanesulfonate

(3S,4R,5S)-1-benzyl-3-(hydroxymethyl)piperidine-3,4,5-triol hydrochloride

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