(E)-1-(3-chloro-1-(4-methoxyphenyl)-5-(4-nitrophenyl)pentan-3-yl)-2-p-tolyldiazene

Base Information

Chemical Name:(E)-1-(3-chloro-1-(4-methoxyphenyl)-5-(4-nitrophenyl)pentan-3-yl)-2-p-tolyldiazene
CAS No.:1381772-58-2
Molecular Formula:C₂₅H₂₆ClN₃O₃
Molecular Weight:451.953
Hs Code.:

Synonyms:(E)-1-(3-chloro-1-(4-methoxyphenyl)-5-(4-nitrophenyl)pentan-3-yl)-2-p-tolyldiazene

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Chemical Property of (E)-1-(3-chloro-1-(4-methoxyphenyl)-5-(4-nitrophenyl)pentan-3-yl)-2-p-tolyldiazene

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Technology Process of (E)-1-(3-chloro-1-(4-methoxyphenyl)-5-(4-nitrophenyl)pentan-3-yl)-2-p-tolyldiazene

There total 2 articles about (E)-1-(3-chloro-1-(4-methoxyphenyl)-5-(4-nitrophenyl)pentan-3-yl)-2-p-tolyldiazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1381772-20-8
(E)-1-(1-(4-methoxyphenyl)-5-(4-nitrophenyl)pentan-3-ylidene)-2-p-tolylhydrazine

: 1381772-58-2
(E)-1-(3-chloro-1-(4-methoxyphenyl)-5-(4-nitrophenyl)pentan-3-yl)-2-p-tolyldiazene

Guidance literature:: (E)-1-(1-(4-methoxyphenyl)-5-(4-nitrophenyl)pentan-3-ylidene)-2-p-tolylhydrazine; With oxalyl dichloride; dimethyl sulfoxide; In tetrahydrofuran; at -78 - -55 ℃; for 0.166667h; Inert atmosphere;

With triethylamine; In tetrahydrofuran; at 25 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1021/ja303054c

Reference yield:

: 1381772-03-7
1-(4-methoxyphenyl)-5-(4-nitrophenyl)pentan-3-one

: 1381772-58-2
(E)-1-(3-chloro-1-(4-methoxyphenyl)-5-(4-nitrophenyl)pentan-3-yl)-2-p-tolyldiazene

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 17 h / Molecular sieve; Inert atmosphere; Reflux

2.1: oxalyl dichloride; dimethyl sulfoxide / tetrahydrofuran / 0.17 h / -78 - -55 °C / Inert atmosphere

2.2: 0.08 h / 25 °C / Inert atmosphere

With oxalyl dichloride; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja303054c

Reference yield: 92.0%

: 1381772-58-2
(E)-1-(3-chloro-1-(4-methoxyphenyl)-5-(4-nitrophenyl)pentan-3-yl)-2-p-tolyldiazene

: 1381772-78-6
5-(4-methoxyphenyl)-3-(4-nitrophenethyl)-1-p-tolyl-4,5-dihydro-1H-pyrazole

Guidance literature:: (E)-1-(3-chloro-1-(4-methoxyphenyl)-5-(4-nitrophenyl)pentan-3-yl)-2-p-tolyldiazene; With aluminum (III) chloride; In dichloromethane; at -60 ℃; for 4h; Inert atmosphere;

With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja303054c