(3-fluorobenzyl)tributyltin

Base Information

Chemical Name:(3-fluorobenzyl)tributyltin
CAS No.:86633-11-6
Molecular Formula:C₁₉H₃₃FSn
Molecular Weight:399.179
Hs Code.:

Synonyms:(3-fluorobenzyl)tributyltin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3-fluorobenzyl)tributyltin

Chemical Property:

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Technology Process of (3-fluorobenzyl)tributyltin

There total 1 articles about (3-fluorobenzyl)tributyltin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1461-22-9
tributyltin chloride

: 7439-95-4
magnesium

: 456-41-7
1-(Bromomethyl)-3-fluorobenzene

: 86633-11-6
(3-fluorobenzyl)tributyltin

Guidance literature:: In diethyl ether; benzene; to mixt. of Mg turnings in ether added substituted benzyl halide at such rate to maintain gentle reflux, when addn. was comlete, mixt. heated at reflux temp. for 1 h, cooled to room temp., added Bu3SnCl in benzene, mixt. heated at reflux temp. for 12 h; added satd. NH4Cl and water, aq. layer sepd., washed with ether, combined org. layers treated with anhyd. NH3 gas for 20 min, filtered, mother liquor washed with water and brine, dried over Na2SO4, concd., distd. under reduced pressure, elem. anal.;
DOI:10.1021/ja00357a026

Reference yield: 70.0%

: 86633-11-6
(3-fluorobenzyl)tributyltin

: 1189797-63-4
9-bromo-2-(4-methylphenyl)-2,6-dihydro[1,2,4]triazolo-[4,3-c]quinazoline-3,5-dione

: 1189797-77-0
9-(3-fluorobenzyl)-2-(4-methylphenyl)-2,6-dihydro-[1,2,4]triazolo[4,3-c]quinazoline-3,5-dione

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In N,N-dimethyl-formamide; at 110 ℃; for 18h; Inert atmosphere; Sealed tube;
DOI:10.1016/j.bmc.2010.11.050