1-(Pyridin-1-ium-1-ylmethyl)pyridin-1-ium diiodide

Base Information

• Chemical Name: 1-(Pyridin-1-ium-1-ylmethyl)pyridin-1-ium diiodide
• CAS No.: 32405-50-8
• Molecular Formula: C11H12 N2 . 2 I
• Molecular Weight: 426.039
• Hs Code.: 2933399090
• DSSTox Substance ID: DTXSID00369583
• Mol file: 32405-50-8.mol

Synonyms:32405-50-8;1,1-METHYLENEDIPYRIDINIUM DIIODIDE;1-(pyridin-1-ium-1-ylmethyl)pyridin-1-ium diiodide;dipyridiniomethan-diiodid;DTXSID00369583;HMS1530D13;CCG-55689;AKOS001046026;1,1'-Methylenedi(pyridin-1-ium) diiodide;FT-0606158;1-(pyridin-1-ium-1-ylmethyl)pyridin-1-ium;diiodide;SR-01000644703-1

Chemical Property of 1-(Pyridin-1-ium-1-ylmethyl)pyridin-1-ium diiodide

Chemical Property:

• PSA: 7.76000
• LogP: -5.22460
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 425.90899
• Heavy Atom Count: 15
• Complexity: 119

Purity/Quality:

99%min ^*data from raw suppliers

1-(1-PYRIDINIUMYLMETHYL)PYRIDINIUM DIIODIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=[N+](C=C1)C[N+]2=CC=CC=C2.[I-].[I-]

Technology Process of 1-(Pyridin-1-ium-1-ylmethyl)pyridin-1-ium diiodide

There total 11 articles about 1-(Pyridin-1-ium-1-ylmethyl)pyridin-1-ium diiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(6-bromonaphthalen-2-yl)ethanone (1590-25-6) → 6-bromo-2-naphthoic acid (5773-80-8) + 1,1-bis(pyridinium)methane diiodide (32405-50-8)

Guidance literature:

With pyridine; water; iodine; In methanol; at 30 ℃; Kinetics; Mechanism; Thermodynamic data; other temperatures; ΔH(excit.);

Reference yield:

methyl 2-naphthyl ketone (93-08-3) → 1,1-bis(pyridinium)methane diiodide (32405-50-8) + naphthalene-2-carboxylate (93-09-4)

Guidance literature:

With pyridine; water; iodine; In methanol; at 30 ℃; Kinetics; Mechanism; Thermodynamic data; various percentage of methanol and water, other temperatures, heterocyclic bases; influence of dielectric constant of the medium, ΔH(excit.);

Reference yield:

1'-naphthacetophenone (941-98-0) → 1-naphthalenecarboxylic acid (86-55-5) + 1,1-bis(pyridinium)methane diiodide (32405-50-8)

Guidance literature:

With pyridine; water; iodine; In methanol; at 30 ℃; Kinetics; Mechanism; Thermodynamic data; various percentage of methanol and water, other temperatures, heterocyclic bases; influence of dielectric constant of the medium, ΔH(excit.);

upstream raw materials:

1'-naphthacetophenone

6-methoxy-2-acetylnaphthalene

6-methyl-2-acetonaphthone

2-acetyl-6-fluoronaphthalene

Downstream raw materials:

(CH₂(NC₅H₅)2)⁽²⁺⁾*[ReCl₅I]^(2-)=[(CH₂(NC₅H₅)2)][ReCl₅I]

Refernces