Technology Process of C20H21N3O5
There total 6 articles about C20H21N3O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Methyltriphenylphosphonium bromide;
With
tert-Amyl alcohol; sodium hydride;
In
tetrahydrofuran;
at 20 ℃;
for 2h;
Inert atmosphere;
C19H19N3O6;
In
tetrahydrofuran;
at 20 ℃;
for 0.5h;
Inert atmosphere;
DOI:10.1016/j.ejmech.2011.01.005
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: toluene-4-sulfonic acid / acetone / 6 h
2.1: dipyridinium dichromate; acetic anhydride / dichloromethane / 1 h / 20 °C / Inert atmosphere
3.1: tert-Amyl alcohol; sodium hydride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
3.2: 0.5 h / 20 °C / Inert atmosphere
With
dipyridinium dichromate; tert-Amyl alcohol; acetic anhydride; sodium hydride; toluene-4-sulfonic acid;
In
tetrahydrofuran; dichloromethane; acetone;
3.2: Wittig reaction;
DOI:10.1016/j.ejmech.2011.01.005
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: dipyridinium dichromate; acetic anhydride / dichloromethane / 1 h / 20 °C / Inert atmosphere
2.1: tert-Amyl alcohol; sodium hydride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
2.2: 0.5 h / 20 °C / Inert atmosphere
With
dipyridinium dichromate; tert-Amyl alcohol; acetic anhydride; sodium hydride;
In
tetrahydrofuran; dichloromethane;
2.2: Wittig reaction;
DOI:10.1016/j.ejmech.2011.01.005