1,2-bis(5-hydroxy-3-oxa-1-pentyloxy)benzene ditosylate

Base Information

Chemical Name:1,2-bis(5-hydroxy-3-oxa-1-pentyloxy)benzene ditosylate
CAS No.:41024-87-7
Molecular Formula:C₂₈H₃₄O₁₀S₂
Molecular Weight:594.704
Hs Code.:

Synonyms:1,2-bis(5-hydroxy-3-oxa-1-pentyloxy)benzene ditosylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-bis(5-hydroxy-3-oxa-1-pentyloxy)benzene ditosylate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of 1,2-bis(5-hydroxy-3-oxa-1-pentyloxy)benzene ditosylate

There total 5 articles about 1,2-bis(5-hydroxy-3-oxa-1-pentyloxy)benzene ditosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 41757-99-7
1,2-bis[2-(2-hydroxyethoxy)ethoxy]benzene

: 98-59-9
p-toluenesulfonyl chloride

: 41024-87-7
1,2-bis(5-hydroxy-3-oxa-1-pentyloxy)benzene ditosylate

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; at 0 ℃; for 2h;
DOI:10.1016/j.tet.2009.07.006

Reference yield:

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 41024-87-7
1,2-bis(5-hydroxy-3-oxa-1-pentyloxy)benzene ditosylate

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH / butan-1-ol / 48 h / Heating

2: NaOH / tetrahydrofuran; H₂O / 4 h / 0 °C

With sodium hydroxide; In tetrahydrofuran; water; butan-1-ol;
DOI:10.1016/j.tetlet.2006.09.161

Reference yield:

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 41024-87-7
1,2-bis(5-hydroxy-3-oxa-1-pentyloxy)benzene ditosylate

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NaOH / 1) n-BuOH, reflux, 2) 16 h, reflux

2: 63 percent / pyridine

With sodium hydroxide; In pyridine;