2,5,11,14-Tetraoxa-8-azoniabicyclo[13.4.0]nonadeca-1(19),15,17-triene

Base Information

Chemical Name:2,5,11,14-Tetraoxa-8-azoniabicyclo[13.4.0]nonadeca-1(19),15,17-triene
CAS No.:54533-83-4
Molecular Formula:C14H21 N O4
Molecular Weight:267.325
Hs Code.:2934999090
DSSTox Substance ID:DTXSID40428108
Wikidata:Q82240893
Mol file:54533-83-4.mol

Synonyms:2,5,11,14-tetraoxa-8-azoniabicyclo[13.4.0]nonadeca-1(19),15,17-triene;54533-83-4;DTXSID40428108

Suppliers and Price of 2,5,11,14-Tetraoxa-8-azoniabicyclo[13.4.0]nonadeca-1(19),15,17-triene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
BENZOAZA-15-CROWN-5 95.00%
5MG
$ 499.30

Total 6 raw suppliers

Chemical Property of 2,5,11,14-Tetraoxa-8-azoniabicyclo[13.4.0]nonadeca-1(19),15,17-triene

Chemical Property:

Vapor Pressure:7.56E-07mmHg at 25°C
Melting Point:147-149oC
Refractive Index:1.5280 (estimate)
Boiling Point:407.4°Cat760mmHg
Flash Point:167.9°C
PSA：53.53000
Density:g/cm³
LogP:1.62360
XLogP3:0.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:268.15488318
Heavy Atom Count:19
Complexity:206

Purity/Quality:

98%Min ^*data from raw suppliers

BENZOAZA-15-CROWN-5 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COCCOC2=CC=CC=C2OCCOCC[NH2+]1

Technology Process of 2,5,11,14-Tetraoxa-8-azoniabicyclo[13.4.0]nonadeca-1(19),15,17-triene

There total 6 articles about 2,5,11,14-Tetraoxa-8-azoniabicyclo[13.4.0]nonadeca-1(19),15,17-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 107102-14-7
2,3-benzo-10-benzyl-10-aza-1,4,7,13-tetraoxa-2-cyclopentadecene

: 54533-83-4
benzo-10-aza-15-crown-5

Guidance literature:: With hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In ethanol; for 6h; Heating;
DOI:10.1021/jo0107148

Reference yield: 40.0%

bis(o-phenylene)glycol ditosylate: 54535-06-7
bis(o-phenylene)glycol ditosylate

: 111-42-2
2,2'-iminobis[ethanol]

: 54533-83-4
benzo-10-aza-15-crown-5

Guidance literature:: With sodium; In tert-butyl alcohol; for 17h; Heating;

Reference yield:

bis(o-phenylene)glycol ditosylate: 54535-06-7
bis(o-phenylene)glycol ditosylate

: 54533-83-4
benzo-10-aza-15-crown-5

Guidance literature:: Multi-step reaction with 2 steps

1: 32 percent / sodium hydride / tetrahydrofuran / 45 h / Heating

2: 71 percent / p-toluenesulfonic acid; hydrogen / palladium/charcoal / ethanol / 6 h / Heating

With hydrogen; sodium hydride; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1021/jo0107148