Technology Process of C22H24O4
There total 6 articles about C22H24O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C15H18O4;
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
at 0 ℃;
for 0.5h;
benzyl bromide;
In
N,N-dimethyl-formamide; mineral oil;
at 0 - 20 ℃;
DOI:10.1021/ol1031409
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: ozone / methanol; dichloromethane / -78 °C
1.2: -78 - 0 °C
2.1: 1H-imidazole / tetrahydrofuran; dichloromethane / 1.33 h / 20 °C
3.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0.67 h / 20 °C / Molecular sieve
4.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / 0 °C
4.2: 12 h / 20 °C
5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C
6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C
6.2: 0 - 20 °C
With
1H-imidazole; n-butyllithium; tetrapropylammonium perruthennate; tetrabutyl ammonium fluoride; sodium hydride; ozone; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; mineral oil;
4.1: Wittig methylenation / 4.2: Wittig methylenation;
DOI:10.1021/ol1031409
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C
2.2: 0 - 20 °C
With
tetrabutyl ammonium fluoride; sodium hydride;
In
tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol1031409
