E,Z-3-benzyl-5-(4-bromobenzoylmethylene)-4-oxo-2-thioxo-1,3-thiazolidine

Base Information

Chemical Name:E,Z-3-benzyl-5-(4-bromobenzoylmethylene)-4-oxo-2-thioxo-1,3-thiazolidine
CAS No.:133901-80-1
Molecular Formula:C₁₉H₁₅NO₂S₂
Molecular Weight:353.466
Hs Code.:

Synonyms:E,Z-3-benzyl-5-(4-bromobenzoylmethylene)-4-oxo-2-thioxo-1,3-thiazolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of E,Z-3-benzyl-5-(4-bromobenzoylmethylene)-4-oxo-2-thioxo-1,3-thiazolidine

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Technology Process of E,Z-3-benzyl-5-(4-bromobenzoylmethylene)-4-oxo-2-thioxo-1,3-thiazolidine

There total 4 articles about E,Z-3-benzyl-5-(4-bromobenzoylmethylene)-4-oxo-2-thioxo-1,3-thiazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 7309-26-4
3-benzyl-5-[2-(4-methylphenyl)-2-oxoethyl]-4-oxo-2-thioxo-1,3-thiazolidine

: 133901-80-1
E,Z-3-benzyl-5-(4-bromobenzoylmethylene)-4-oxo-2-thioxo-1,3-thiazolidine

Guidance literature:: With bromine; acetic acid; for 0.0833333h; Heating;
DOI:10.1246/bcsj.64.750

Reference yield:

: 41270-27-3
N-benzyl-dithiocarbamic acid ammonium salt

: 133901-80-1
E,Z-3-benzyl-5-(4-bromobenzoylmethylene)-4-oxo-2-thioxo-1,3-thiazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: conc. HCl / ethanol / 0.5 h / 20 °C

2: Br₂ / acetic acid / 0.08 h / Heating

With hydrogenchloride; bromine; In ethanol; acetic acid;
DOI:10.3390/60600510

Reference yield:

: 35513-41-8
cis-3-Toluoloylacrylsaeure

: 133901-80-1
E,Z-3-benzyl-5-(4-bromobenzoylmethylene)-4-oxo-2-thioxo-1,3-thiazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: conc. HCl / ethanol / 0.5 h / 20 °C

2: Br₂ / acetic acid / 0.08 h / Heating

With hydrogenchloride; bromine; In ethanol; acetic acid;
DOI:10.3390/60600510