[(4-Chloro-phenylcarbamoyl)-methyl]-dithiocarbamic acid benzyl ester

Base Information

• Chemical Name: [(4-Chloro-phenylcarbamoyl)-methyl]-dithiocarbamic acid benzyl ester
• CAS No.: 71011-43-3
• Molecular Formula: C₁₆H₁₅ClN₂OS₂
• Molecular Weight: 350.893
• Mol file: 71011-43-3.mol

Synonyms:[(4-Chloro-phenylcarbamoyl)-methyl]-dithiocarbamic acid benzyl ester

Chemical Property of [(4-Chloro-phenylcarbamoyl)-methyl]-dithiocarbamic acid benzyl ester

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of [(4-Chloro-phenylcarbamoyl)-methyl]-dithiocarbamic acid benzyl ester

There total 3 articles about [(4-Chloro-phenylcarbamoyl)-methyl]-dithiocarbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2-(((benzylthio)carbonothioyl)amino)acetic acid (4596-57-0) + 4-chloro-aniline (106-47-8) → [(4-Chloro-phenylcarbamoyl)-methyl]-dithiocarbamic acid benzyl ester (71011-43-3)

Guidance literature:

In neat (no solvent); at 100 ℃;

DOI:10.1039/c3ra44552f

Reference yield:

benzyl chloride (100-44-7) → [(4-Chloro-phenylcarbamoyl)-methyl]-dithiocarbamic acid benzyl ester (71011-43-3)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide / methanol

2: neat (no solvent) / 100 °C

With sodium hydroxide; In methanol;

DOI:10.1039/c3ra44552f

Reference yield:

→ [(4-Chloro-phenylcarbamoyl)-methyl]-dithiocarbamic acid benzyl ester (71011-43-3)

Guidance literature:

Azolon 2, p-Chlorphenylamin;

DOI:10.1016/S0040-4039(01)85961-X

upstream raw materials:

benzyl chloride

2-(((benzylthio)carbonothioyl)amino)acetic acid

4-chloro-aniline