C₂₁H₂₄N₂O₅

Base Information

Chemical Name:C₂₁H₂₄N₂O₅
CAS No.:888970-78-3
Molecular Formula:C₂₁H₂₄N₂O₅
Molecular Weight:384.432
Hs Code.:

C<sub>21</sub>H<sub>24</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₁H₂₄N₂O₅

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Chemical Property of C₂₁H₂₄N₂O₅

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Technology Process of C₂₁H₂₄N₂O₅

There total 4 articles about C₂₁H₂₄N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1048653-48-0
C₁₁H₁₅NO₂*ClH

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 888970-78-3
C₂₁H₂₄N₂O₅

Guidance literature:: C₁₁H₁₅NO₂*ClH; N-(Benzyloxycarbonyl)glycine; With HATU; In dichloromethane; at 0 ℃; for 0.333333h; Inert atmosphere;

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 36h; Inert atmosphere;
DOI:10.1016/j.tet.2011.06.032

Reference yield:

: (R)-(+)-α-4-methylphenylalanine

: 888970-78-3
C₂₁H₂₄N₂O₅

Guidance literature:: Multi-step reaction with 2 steps

1.1: thionyl chloride / -15 °C / Reflux

1.2: 2 h / 20 °C

2.1: HATU / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

2.2: 36 h / 20 °C / Inert atmosphere

With thionyl chloride; HATU; In dichloromethane;
DOI:10.1016/j.tet.2011.06.032

Reference yield:

: 122-00-9
para-methylacetophenone

: 888970-78-3
C₂₁H₂₄N₂O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: ammonium hydroxide / ethanol / 4 h / 60 - 65 °C

1.3: Auto-seeded programmed polythermic preferential crystallization; Resolution of racemate

2.1: sodium hydroxide / water / 72 h / Reflux

3.1: thionyl chloride / -15 °C / Reflux

3.2: 2 h / 20 °C

4.1: HATU / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

4.2: 36 h / 20 °C / Inert atmosphere

With ammonium hydroxide; thionyl chloride; HATU; sodium hydroxide; In ethanol; dichloromethane; water; 1.1: Bucherer-Bergs reaction;
DOI:10.1016/j.tet.2011.06.032