C₅₁H₇₃NO₁₈Si

Base Information

Chemical Name:C₅₁H₇₃NO₁₈Si
CAS No.:871130-06-2
Molecular Formula:C₅₁H₇₃NO₁₈Si
Molecular Weight:1016.22
Hs Code.:

C<sub>51</sub>H<sub>73</sub>NO<sub>18</sub>Si

Synonyms:C₅₁H₇₃NO₁₈Si

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Chemical Property of C₅₁H₇₃NO₁₈Si

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Technology Process of C₅₁H₇₃NO₁₈Si

There total 6 articles about C₅₁H₇₃NO₁₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 675584-89-1
C₄₅H₅₉NO₁₈

: 18162-48-6
tert-butyldimethylsilyl chloride

: 871130-06-2
C₅₁H₇₃NO₁₈Si

Guidance literature:: With dmap; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmcl.2005.08.066

Reference yield:

: 675584-85-7
C₃₉H₅₀O₁₄Si

: 871130-06-2
C₅₁H₇₃NO₁₈Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: 76 percent / Et₄N(BH₄) / methanol / 2.5 h / -40 - 0 °C

2.1: DMAP; EDCI / CH₂Cl₂ / 1.5 h / 20 °C

3.1: HF; pyridine / acetonitrile / 2 h / 20 °C

3.2: 248 mg / AcCl; MeOH / CH₂Cl₂ / 20 °C

4.1: 90 percent / DMAP / CH₂Cl₂ / 20 °C

With pyridine; dmap; hydrogen fluoride; tetraethylammonium borohydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2005.08.066

Reference yield:

: 675584-84-6
C₃₈H₅₂O₁₃Si

: 871130-06-2
C₅₁H₇₃NO₁₈Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: 230 mg / imidazole / CH₂Cl₂ / 1.5 h / 40 °C

2.1: 76 percent / Et₄N(BH₄) / methanol / 2.5 h / -40 - 0 °C

3.1: DMAP; EDCI / CH₂Cl₂ / 1.5 h / 20 °C

4.1: HF; pyridine / acetonitrile / 2 h / 20 °C

4.2: 248 mg / AcCl; MeOH / CH₂Cl₂ / 20 °C

5.1: 90 percent / DMAP / CH₂Cl₂ / 20 °C

With pyridine; 1H-imidazole; dmap; hydrogen fluoride; tetraethylammonium borohydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2005.08.066