ethylene (3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate) (2-methyl-5,5-diphenyl-4,5-dihydrofuran-3-carboxylate)

Base Information

• Chemical Name: ethylene (3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate) (2-methyl-5,5-diphenyl-4,5-dihydrofuran-3-carboxylate)
• CAS No.: 174498-18-1
• Molecular Formula: C₃₈H₃₆O₈
• Molecular Weight: 620.699
• Mol file: 174498-18-1.mol

Synonyms:ethylene (3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate) (2-methyl-5,5-diphenyl-4,5-dihydrofuran-3-carboxylate)

Chemical Property of ethylene (3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate) (2-methyl-5,5-diphenyl-4,5-dihydrofuran-3-carboxylate)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethylene (3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate) (2-methyl-5,5-diphenyl-4,5-dihydrofuran-3-carboxylate)

There total 5 articles about ethylene (3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate) (2-methyl-5,5-diphenyl-4,5-dihydrofuran-3-carboxylate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

1,1-Diphenylethylene (530-48-3) + 2-(3-oxobutanoyloxy)ethyl-2-methyl-5,5-diphenyl-4,5-dihydrofuran-3-carboxylate (174498-24-9) → 2-hydroxyethyl 2-methyl-5,5-diphenyl-4,5-dihydrofuran-3-carboxylate + ethylene (3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate) (2-methyl-5,5-diphenyl-4,5-dihydrofuran-3-carboxylate) (174498-18-1)

Guidance literature:

With manganese triacetate; In acetic acid; at 23 ℃; for 20h;

Reference yield: 48.0%

1,1-Diphenylethylene (530-48-3) + 2-(3-oxobutanoyloxy)ethyl 3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate (174498-07-8) → ethylene di(2-methyl-5,5-diphenyl-4,5-dihydrofuran-3-carboxylate) (174498-25-0) + ethylene (3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate) (2-methyl-5,5-diphenyl-4,5-dihydrofuran-3-carboxylate) (174498-18-1)

Guidance literature:

With manganese triacetate; In acetic acid; at 23 ℃; for 20h;

Reference yield: 38.0%

1,1-Diphenylethylene (530-48-3) + ethane-1,2-diylbis(3-oxobutanoate) (5459-04-1) → ethylene (3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate) (2-methyl-5,5-diphenyl-4,5-dihydrofuran-3-carboxylate) (174498-18-1) + ethylene di(3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate) (174498-08-9)

Guidance literature:

With manganese(II) acetate; manganese triacetate; In acetic acid; at 23 ℃; for 24h;

upstream raw materials:

1,1-Diphenylethylene

ethane-1,2-diylbis(3-oxobutanoate)

2-(3-oxobutanoyloxy)ethyl-2-methyl-5,5-diphenyl-4,5-dihydrofuran-3-carboxylate

2-(3-oxobutanoyloxy)ethyl 3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate