2-(3-oxobutanoyloxy)ethyl 3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate

Base Information

• Chemical Name: 2-(3-oxobutanoyloxy)ethyl 3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate
• CAS No.: 174498-07-8
• Molecular Formula: C₂₄H₂₆O₈
• Molecular Weight: 442.466

Synonyms:2-(3-oxobutanoyloxy)ethyl 3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate

Chemical Property of 2-(3-oxobutanoyloxy)ethyl 3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate

Chemical Property:

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Technology Process of 2-(3-oxobutanoyloxy)ethyl 3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate

There total 1 articles about 2-(3-oxobutanoyloxy)ethyl 3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

1,1-Diphenylethylene (530-48-3) + ethane-1,2-diylbis(3-oxobutanoate) (5459-04-1) → 2-hydroxyethyl-3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate + 2-(3-oxobutanoyloxy)ethyl 3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate (174498-07-8) + ethylene di(3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate) (174498-08-9)

Guidance literature:

With manganese(II) acetate; manganese triacetate; In acetic acid; at 23 ℃; for 2.5h;

Reference yield: 48.0%

1,1-Diphenylethylene (530-48-3) + 2-(3-oxobutanoyloxy)ethyl 3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate (174498-07-8) → ethylene di(2-methyl-5,5-diphenyl-4,5-dihydrofuran-3-carboxylate) (174498-25-0) + ethylene (3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate) (2-methyl-5,5-diphenyl-4,5-dihydrofuran-3-carboxylate) (174498-18-1)

Guidance literature:

With manganese triacetate; In acetic acid; at 23 ℃; for 20h;

Reference yield: 42.0%

1,1-Diphenylethylene (530-48-3) + 2-(3-oxobutanoyloxy)ethyl 3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate (174498-07-8) → benzophenone (119-61-9) + 2-hydroxyethyl-3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate + ethylene di(3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate) (174498-08-9)

Guidance literature:

With manganese triacetate; In acetic acid; at 23 ℃; for 20h;

upstream raw materials:

1,1-Diphenylethylene

ethane-1,2-diylbis(3-oxobutanoate)

Downstream raw materials:

benzophenone

ethylene di(3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate)

ethylene di(2-methyl-5,5-diphenyl-4,5-dihydrofuran-3-carboxylate)

ethylene (3-hydroxy-3-methyl-6,6-diphenyl-1,2-dioxane-4-carboxylate) (2-methyl-5,5-diphenyl-4,5-dihydrofuran-3-carboxylate)

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