C₁₉H₂₁N₃O₄

Base Information

Chemical Name:C₁₉H₂₁N₃O₄
CAS No.:1407163-94-3
Molecular Formula:C₁₉H₂₁N₃O₄
Molecular Weight:355.393
Hs Code.:

C<sub>19</sub>H<sub>21</sub>N<sub>3</sub>O<sub>4</sub>

Synonyms:C₁₉H₂₁N₃O₄

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Chemical Property of C₁₉H₂₁N₃O₄

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Technology Process of C₁₉H₂₁N₃O₄

There total 3 articles about C₁₉H₂₁N₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 609-73-4
o-nitroiodobenzene

: 1407163-93-2
C₁₃H₁₇IN₂O₂

: 1407163-94-3
C₁₉H₂₁N₃O₄

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper; In dimethyl sulfoxide; at 70 ℃; for 0.5h;
DOI:10.1021/ol3026846

Reference yield:

: 1407163-91-0
C₁₃H₂₀N₂O

: 1407163-94-3
C₁₉H₂₁N₃O₄

Guidance literature:: Multi-step reaction with 3 steps

1: manganese(III) triacetate dihydrate; tert.-butylhydroperoxide / ethyl acetate; decane / 16.5 h / 18 °C / Molecular sieve

2: iodine / chloroform; pyridine / 16.2 h / 18 °C / Inert atmosphere

3: copper; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / dimethyl sulfoxide / 0.5 h / 70 °C

With tert.-butylhydroperoxide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; iodine; manganese(III) triacetate dihydrate; copper; In pyridine; decane; chloroform; dimethyl sulfoxide; ethyl acetate; 3: |Ullmann Condensation;
DOI:10.1021/ol3026846

Reference yield:

: 1407163-92-1
C₁₃H₁₈N₂O₂

: 1407163-94-3
C₁₉H₂₁N₃O₄

Guidance literature:: Multi-step reaction with 2 steps

1: iodine / chloroform; pyridine / 16.2 h / 18 °C / Inert atmosphere

2: copper; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / dimethyl sulfoxide / 0.5 h / 70 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; iodine; copper; In pyridine; chloroform; dimethyl sulfoxide; 2: |Ullmann Condensation;
DOI:10.1021/ol3026846