C₁₅H₁₂F₃NO₃

Base Information

Chemical Name:C₁₅H₁₂F₃NO₃
CAS No.:1276039-98-5
Molecular Formula:C₁₅H₁₂F₃NO₃
Molecular Weight:311.26
Hs Code.:

C<sub>15</sub>H<sub>12</sub>F<sub>3</sub>NO<sub>3</sub>

Synonyms:C₁₅H₁₂F₃NO₃

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Chemical Property of C₁₅H₁₂F₃NO₃

Chemical Property:

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Technology Process of C₁₅H₁₂F₃NO₃

There total 8 articles about C₁₅H₁₂F₃NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₁₂F₃NO₃

: 1276039-98-5
C₁₅H₁₂F₃NO₃

Guidance literature:: With sulfuric acid; dihydrogen peroxide; In water; at 0 - 20 ℃; for 1h;

Reference yield:

: 124700-41-0
2-fluoro-5-iodobenzoic acid

: 1276039-98-5
C₁₅H₁₂F₃NO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide; acetonitrile / 20 °C

2.1: bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 2 h / Reflux

3.1: sodium periodate; osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol / 20 °C

4.1: potassium carbonate / dimethyl sulfoxide / 28 h / 90 - 120 °C

4.2: 1 h / 50 °C

5.1: sulfuric acid; dihydrogen peroxide / water / 1 h / 0 - 20 °C

With sodium periodate; osmium(VIII) oxide; sulfuric acid; dihydrogen peroxide; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; 1,4-dioxane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;

Reference yield:

: 625471-27-4
methyl 2-fluoro-5-iodo-benzoate

: 1276039-98-5
C₁₅H₁₂F₃NO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 2 h / Reflux

2.1: sodium periodate; osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol / 20 °C

3.1: potassium carbonate / dimethyl sulfoxide / 28 h / 90 - 120 °C

3.2: 1 h / 50 °C

4.1: sulfuric acid; dihydrogen peroxide / water / 1 h / 0 - 20 °C

With sodium periodate; osmium(VIII) oxide; sulfuric acid; dihydrogen peroxide; potassium carbonate; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; 1,4-dioxane; water; dimethyl sulfoxide; tert-butyl alcohol;