(Z)-2-[-2-(3-isopropoxy-4-methoxystyryl)-4-isopropoxy-5-methoxyphenyl]-N-hydroxyethanamine

Base Information

Chemical Name:(Z)-2-[-2-(3-isopropoxy-4-methoxystyryl)-4-isopropoxy-5-methoxyphenyl]-N-hydroxyethanamine
CAS No.:1108621-35-7
Molecular Formula:C₂₄H₃₃NO₅
Molecular Weight:415.53
Hs Code.:

Synonyms:(Z)-2-[-2-(3-isopropoxy-4-methoxystyryl)-4-isopropoxy-5-methoxyphenyl]-N-hydroxyethanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-[-2-(3-isopropoxy-4-methoxystyryl)-4-isopropoxy-5-methoxyphenyl]-N-hydroxyethanamine

Chemical Property:

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Technology Process of (Z)-2-[-2-(3-isopropoxy-4-methoxystyryl)-4-isopropoxy-5-methoxyphenyl]-N-hydroxyethanamine

There total 9 articles about (Z)-2-[-2-(3-isopropoxy-4-methoxystyryl)-4-isopropoxy-5-methoxyphenyl]-N-hydroxyethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1108621-60-8
2-(2-(3-isopropoxy-4-methoxystyryl)-4-isopropoxy-5-methoxyphenyl)ethoxime

: 1108621-35-7
(Z)-2-[-2-(3-isopropoxy-4-methoxystyryl)-4-isopropoxy-5-methoxyphenyl]-N-hydroxyethanamine

Guidance literature:: With hydrogenchloride; sodium cyanoborohydride; In methanol; water; for 0.5h; Inert atmosphere;

Reference yield:

: 56517-33-0
4-isopropoxy-2-bromo-5-methoxybenzaldehyde

: 1108621-35-7
(Z)-2-[-2-(3-isopropoxy-4-methoxystyryl)-4-isopropoxy-5-methoxyphenyl]-N-hydroxyethanamine

Guidance literature:: Multi-step reaction with 5 steps

1: trans-bis(triphenylphosphine)palladium dichloride; copper(l) iodide; triethylamine / 24 h / 20 °C

2: acetic acid / 4 h / 100 °C

3: tin(ll) chloride / ethyl acetate / 10 h / 20 °C

4: hydrogen / ethyl acetate / 5 h / 760.05 Torr

5: sodium cyanoborohydride / methanol / 1 h / 20 °C / pH Ca_. 3

With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; hydrogen; sodium cyanoborohydride; acetic acid; triethylamine; tin(ll) chloride; In methanol; ethyl acetate; 1: |Sonogashira Cross-Coupling;
DOI:10.1021/jo4023149

Reference yield:

: 34123-66-5
O-isopropylisovanillin

: 1108621-35-7
(Z)-2-[-2-(3-isopropoxy-4-methoxystyryl)-4-isopropoxy-5-methoxyphenyl]-N-hydroxyethanamine

Guidance literature:: Multi-step reaction with 7 steps

1: zinc; triphenylphosphine / dichloromethane / 1 h / 20 °C

2: n-butyllithium / tetrahydrofuran / 2 h / -78 °C

3: trans-bis(triphenylphosphine)palladium dichloride; copper(l) iodide; triethylamine / 24 h / 20 °C

4: acetic acid / 4 h / 100 °C

5: tin(ll) chloride / ethyl acetate / 10 h / 20 °C

6: hydrogen / ethyl acetate / 5 h / 760.05 Torr

7: sodium cyanoborohydride / methanol / 1 h / 20 °C / pH Ca_. 3

With copper(l) iodide; n-butyllithium; trans-bis(triphenylphosphine)palladium dichloride; hydrogen; sodium cyanoborohydride; acetic acid; triethylamine; triphenylphosphine; tin(ll) chloride; zinc; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; 1: |Corey-Fuchs Alkyne Synthesis / 2: |Corey-Fuchs Alkyne Synthesis / 3: |Sonogashira Cross-Coupling;
DOI:10.1021/jo4023149