C₃₂H₂₇Cl₆N₅O₅

Base Information

Chemical Name:C₃₂H₂₇Cl₆N₅O₅
CAS No.:1591741-80-8
Molecular Formula:C₃₂H₂₇Cl₆N₅O₅
Molecular Weight:774.315
Hs Code.:

C<sub>32</sub>H<sub>27</sub>Cl<sub>6</sub>N<sub>5</sub>O<sub>5</sub>

Synonyms:C₃₂H₂₇Cl₆N₅O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₂H₂₇Cl₆N₅O₅

Chemical Property:

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Technology Process of C₃₂H₂₇Cl₆N₅O₅

There total 6 articles about C₃₂H₂₇Cl₆N₅O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1591741-74-0
C₄₆H₅₁Cl₆N₅O₁₀

: 1591741-80-8
C₃₂H₂₇Cl₆N₅O₅

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In acetonitrile; at -10 - 20 ℃; for 2.33333h; stereoselective reaction; Inert atmosphere;
DOI:10.1021/ml500077j

Reference yield:

: 677299-15-9
3,5-bis-O-(2,4-dichlorophenylmethyl)-1-O-methyl-2-C-methyl-D-ribofuranose

: 1591741-80-8
C₃₂H₂₇Cl₆N₅O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.67 h / 0 °C / Inert atmosphere

1.2: 70 °C / Inert atmosphere

2.1: trifluoroacetic acid; water / 4 h / 0 - 20 °C

3.1: pyridinium chlorochromate / dichloromethane / 48 h / 20 °C

4.1: n-butyllithium / hexane; tetrahydrofuran / 0.25 h / -100 °C

5.1: boron trifluoride diethyl etherate; triethylsilane / acetonitrile / 2.33 h / -10 - 20 °C / Inert atmosphere

With triethylsilane; n-butyllithium; boron trifluoride diethyl etherate; water; sodium hydride; pyridinium chlorochromate; trifluoroacetic acid; In tetrahydrofuran; hexane; dichloromethane; acetonitrile; mineral oil;
DOI:10.1021/ml500077j

Reference yield:

: 1203549-21-6
C₂₈H₂₆Cl₆O₅

: 1591741-80-8
C₃₂H₂₇Cl₆N₅O₅

Guidance literature:: Multi-step reaction with 4 steps

1: trifluoroacetic acid; water / 4 h / 0 - 20 °C

2: pyridinium chlorochromate / dichloromethane / 48 h / 20 °C

3: n-butyllithium / hexane; tetrahydrofuran / 0.25 h / -100 °C

4: boron trifluoride diethyl etherate; triethylsilane / acetonitrile / 2.33 h / -10 - 20 °C / Inert atmosphere

With triethylsilane; n-butyllithium; boron trifluoride diethyl etherate; water; pyridinium chlorochromate; trifluoroacetic acid; In tetrahydrofuran; hexane; dichloromethane; acetonitrile;
DOI:10.1021/ml500077j