C₆₁H₁₁₂O₁₇Si₃

Base Information

Chemical Name:C₆₁H₁₁₂O₁₇Si₃
CAS No.:795290-08-3
Molecular Formula:C₆₁H₁₁₂O₁₇Si₃
Molecular Weight:1201.81
Hs Code.:

C<sub>61</sub>H<sub>112</sub>O<sub>17</sub>Si<sub>3</sub>

Synonyms:C₆₁H₁₁₂O₁₇Si₃

Suppliers and Price of C₆₁H₁₁₂O₁₇Si₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆₁H₁₁₂O₁₇Si₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆₁H₁₁₂O₁₇Si₃

There total 20 articles about C₆₁H₁₁₂O₁₇Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 795290-07-2
C₆₁H₁₁₁IO₁₇Si₃

: 795290-08-3
C₆₁H₁₁₂O₁₇Si₃

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 100 ℃; for 15h;
DOI:10.1002/anie.200460172

Reference yield:

: 795289-92-8
3-O-triethylsilyl-L-olivomycal

: 795290-08-3
C₆₁H₁₁₂O₁₇Si₃

Guidance literature:: Multi-step reaction with 5 steps

1: TMSOTf / diethyl ether / 1 h / -60 - -40 °C

2: NaI / dimethylformamide / 2 h / 90 °C

3: Bu₃SnH; 2,2'-azobis(isobutyronitrile) / toluene / 7 h / 100 °C

4: N-iodosuccinimide; 4-Angstroem molecular sieves / CH₂Cl₂ / 72 h / 0 - 20 °C

5: 96 percent / Bu₃SnH; 2,2'-azobis(isobutyronitrile) / toluene / 15 h / 100 °C

With N-iodo-succinimide; 2,2'-azobis(isobutyronitrile); trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; tri-n-butyl-tin hydride; sodium iodide; In diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/anie.200460172

Reference yield:

: 795289-91-7
(3aR,6S,7S,7aR)-4-Methoxy-6-methyl-2-phenyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-ol

: 795290-08-3
C₆₁H₁₁₂O₁₇Si₃

Guidance literature:: Multi-step reaction with 9 steps

1: 43 percent / tetrahydrofuran / 30 h / 20 °C

2: 4-dimethylaminopyridine / CH₂Cl₂

3: lutidine

4: diisobutylaluminum hydride / CH₂Cl₂ / -60 °C

5: TMSOTf / diethyl ether / 1 h / -60 - -40 °C

6: NaI / dimethylformamide / 2 h / 90 °C

7: Bu₃SnH; 2,2'-azobis(isobutyronitrile) / toluene / 7 h / 100 °C

8: N-iodosuccinimide; 4-Angstroem molecular sieves / CH₂Cl₂ / 72 h / 0 - 20 °C

9: 96 percent / Bu₃SnH; 2,2'-azobis(isobutyronitrile) / toluene / 15 h / 100 °C

With dmap; N-iodo-succinimide; 2,2'-azobis(isobutyronitrile); trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; lutidine; tri-n-butyl-tin hydride; diisobutylaluminium hydride; sodium iodide; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/anie.200460172