C₆₂H₇₆O₁₀

Base Information

• Chemical Name: C₆₂H₇₆O₁₀
• CAS No.: 1558035-01-0
• Molecular Formula: C₆₂H₇₆O₁₀
• Molecular Weight: 981.279
• Mol file: 1558035-01-0.mol

Synonyms:C₆₂H₇₆O₁₀

Chemical Property of C₆₂H₇₆O₁₀

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₂H₇₆O₁₀

There total 11 articles about C₆₂H₇₆O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

C64H80O10 (1558035-00-9) → C62H76O10 (1558035-01-0)

Guidance literature:

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; ethene; In dichloromethane; at 40 ℃; for 2h;

DOI:10.1021/ol5002686

Reference yield:

phthalic anhydride (85-44-9) → C62H76O10 (1558035-01-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: pyridine; dmap / 16 h / 20 °C / Inert atmosphere

2.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere

2.2: 1 h / 20 °C / Inert atmosphere

3.1: ethene; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 2 h / 40 °C

With pyridine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; ethene; 2,4,6-trichlorobenzoyl chloride; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ol5002686

Reference yield:

1-(3',4',6'-tri-O-benzyl-α-D-galactopyranosyl)-2-propene (271246-08-3) → C62H76O10 (1558035-01-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: pyridine; dmap / 16 h / 20 °C / Inert atmosphere

2.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere

2.2: 1 h / 20 °C / Inert atmosphere

3.1: ethene; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 2 h / 40 °C

With pyridine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; ethene; 2,4,6-trichlorobenzoyl chloride; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ol5002686

upstream raw materials:

1-(3',4',6'-tri-O-benzyl-α-D-galactopyranosyl)-2-propene

C₃₈H₃₈O₈

C₆₄H₈₀O₁₀

1-tetradecene

Downstream raw materials:

C₅₄H₇₄O₈

C₆₈H₈₆O₈

C₆₀H₇₈O₇

C₆₉H₈₇NO₇S