3-Benzyloxy-4-methoxybenzylazid

Base Information

Chemical Name:3-Benzyloxy-4-methoxybenzylazid
CAS No.:57535-60-1
Molecular Formula:C₁₅H₁₅N₃O₂
Molecular Weight:269.303
Hs Code.:

Synonyms:3-Benzyloxy-4-methoxybenzylazid

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Chemical Property of 3-Benzyloxy-4-methoxybenzylazid

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Technology Process of 3-Benzyloxy-4-methoxybenzylazid

There total 1 articles about 3-Benzyloxy-4-methoxybenzylazid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1699-38-3
3-benzyloxy-4-methoxy-benzyl chloride

: 57535-60-1
3-Benzyloxy-4-methoxybenzylazid

Guidance literature:: With sodium azide; In acetone;

Reference yield: 83.0%

: 57535-60-1
3-Benzyloxy-4-methoxybenzylazid

: 4-(6-methoxybenzo[d]thiazol-2-yl)-2-nitro-N-(prop-2-ynyl)benzamide

: N-((1-(3-(benzyloxy)-4-methoxybenzyl)-1H-1,2,3-triazol-4-yl)methyl)-4-(6-methoxybenzo[d]thiazol-2-yl)-2-nitrobenzamide

Guidance literature:: 3-Benzyloxy-4-methoxybenzylazid; 4-(6-methoxybenzo[d]thiazol-2-yl)-2-nitro-N-(prop-2-ynyl)benzamide; In water; tert-butyl alcohol;

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃; for 11.3h; regioselective reaction;
DOI:10.1002/jhet.2647