butyl (2E,6E)-7-(2-chlorophenyl)-4-(1,3-dithiolan-2-ylidene)-5-oxohepta-2,6-dienoate

Base Information

Chemical Name:butyl (2E,6E)-7-(2-chlorophenyl)-4-(1,3-dithiolan-2-ylidene)-5-oxohepta-2,6-dienoate
CAS No.:1346757-25-2
Molecular Formula:C₂₀H₂₁ClO₃S₂
Molecular Weight:408.97
Hs Code.:

Synonyms:butyl (2E,6E)-7-(2-chlorophenyl)-4-(1,3-dithiolan-2-ylidene)-5-oxohepta-2,6-dienoate

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Chemical Property of butyl (2E,6E)-7-(2-chlorophenyl)-4-(1,3-dithiolan-2-ylidene)-5-oxohepta-2,6-dienoate

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Technology Process of butyl (2E,6E)-7-(2-chlorophenyl)-4-(1,3-dithiolan-2-ylidene)-5-oxohepta-2,6-dienoate

There total 1 articles about butyl (2E,6E)-7-(2-chlorophenyl)-4-(1,3-dithiolan-2-ylidene)-5-oxohepta-2,6-dienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 141-32-2,9003-49-0
acrylic acid n-butyl ester

: C₁₃H₁₀ClIOS₂

: 1346757-25-2
butyl (2E,6E)-7-(2-chlorophenyl)-4-(1,3-dithiolan-2-ylidene)-5-oxohepta-2,6-dienoate

Guidance literature:: With palladium diacetate; potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 0.75h;
DOI:10.1039/c1cc14916d

Reference yield: 84.0%

: 2999-46-4
Ethyl isocyanoacetate

: 1346757-25-2
butyl (2E,6E)-7-(2-chlorophenyl)-4-(1,3-dithiolan-2-ylidene)-5-oxohepta-2,6-dienoate

: 3-butyl 7a-ethyl 7-(2-chlorophenyl)-4-(1,3-dithiolan-2-ylidene)-5-oxo-3a,4,5,6,7,7a-hexahydro-1H-indole-3,7a-dicarboxylate

Guidance literature:: With sodium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 0.3h; diastereoselective reaction;
DOI:10.1039/c1cc14916d